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网站主页CAS数据库列表 86436-20-6更多图谱双(2-氯苯基)-联苯基-已二炔-二醇(86436-20-6)质谱(MS)

双(2-氯苯基)-联苯基-已二炔-二醇

产品名称 双(2-氯苯基)-联苯基-已二炔-二醇

CAS号86436-20-6

分子式C30H20Cl2O2

分子量483.38

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  • Mass

    MS-IW-4044          
    (-)-1,6-bis(o-chlorophenyl)-1,6-diphenyl-2,4-hexadiyne-1,6-diol
    C30H20Cl2O2         (Mass of molecular ion:    482)
    

       Source Temperature: 180 °C
       Sample Temperature: 170 °C
       Direct, 75 eV
    

          17.0       1.2
          18.0       6.8
          28.0       1.0
          39.0       1.2
          49.0       1.4
          50.0       7.2
          51.0      12.0
          52.0       1.0
          63.0       2.1
          74.0       2.5
          75.0      11.1
          76.0       7.4
          77.0      49.5
          78.0       4.4
          86.0       1.0
          87.0       1.8
          88.0       3.6
          93.5       1.0
          94.0       1.6
          99.0       1.5
         100.0       3.3
         100.5       1.7
         101.0       9.4
         101.5       2.1
         105.0     100.0
         105.5       1.1
         106.0       8.9
         106.5       2.2
         107.0       1.2
         111.0      17.9
         112.0       2.0
         113.0       6.1
         125.0       2.0
         126.0       4.7
         127.0       2.3
         137.0       1.7
         138.0       1.1
         139.0      54.9
         140.0       4.3
         141.0      18.1
         142.0       1.4
         150.0       1.5
         151.0       2.6
         152.0       4.6
         153.0       2.2
         154.0       4.8
         155.0       3.4
         160.0       1.9
         162.0       1.0
         163.0       1.3
         165.0       1.1
         176.0       1.2
         180.0       1.0
         181.0       4.7
         187.0       1.4
         188.0       6.2
         189.0       3.1
         190.0       2.1
         191.0       1.0
         199.0       1.2
         200.0       4.4
         201.0       6.5
         202.0      36.5
         203.0      23.7
         204.0       3.6
         211.0       2.1
         212.0       1.7
         213.0       6.3
         214.0       1.7
         215.0       1.4
         216.0      42.0
         217.0       6.5
         218.0      14.1
         219.0       2.1
         229.0       1.0
         230.0       4.2
         231.0      43.9
         232.0       8.2
         238.0       1.6
         249.0       2.1
         265.0       5.4
         266.0       1.4
         267.0       1.9
         289.0       1.2
         307.0       1.0
         343.0       2.9
         345.0       1.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C30 H20 Cl2 O2 0.038 g : 0.5 ml CDCl3
    (-)-1,6-bis(o-chlorophenyl)-1,6-diphenyl-2,4-hexadiyne-1,6-diol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.885 B 7.473 C 7.48 to 7.46 D 7.272 E 3.26

         Hz     ppm     Int.
    

       3156.13   7.898    214
       3154.66   7.894    181
       3151.25   7.886     65
       3149.90   7.882     67
       3148.80   7.879    203
       3148.32   7.878    225
       3146.48   7.874    202
       2993.04   7.490     60
       2991.70   7.486    319
       2990.48   7.483    136
       2989.50   7.481    216
       2987.55   7.476    140
       2986.45   7.473    147
       2985.47   7.471    201
       2983.64   7.466    446
       2982.06   7.462    411
       2979.98   7.457     44
       2978.88   7.454     50
       2937.62   7.351     78
       2935.91   7.347     59
       2933.59   7.341    210
       2931.76   7.336    216
       2930.79   7.334    201
       2929.20   7.330    449
       2926.76   7.324    295
       2925.05   7.320    530
       2922.97   7.314    712
       2922.49   7.313    709
       2921.26   7.310    756
       2918.21   7.302    391
       2916.38   7.298    166
       2912.11   7.287    273
       2910.28   7.283    300
       2907.84   7.276     78
       2905.40   7.270    141
       2903.93   7.267    119
       2902.95   7.264    198
       2897.22   7.250     83
       2895.51   7.246     73
       1302.73   3.260   1000
    

KBr disc



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