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MassMS-NW-8764 2-phenyl-3-butyn-2-ol C10H10O (Mass of molecular ion: 146)
Source Temperature: 280 °C Sample Temperature: 130 °C Reservoir, 75 eV
18.0 1.0 27.0 1.2 39.0 3.3 43.0 9.0 50.0 4.5 51.0 13.7 52.0 2.4 53.0 76.8 54.0 2.6 62.0 1.4 63.0 3.3 64.0 1.1 65.0 1.1 65.5 3.2 69.0 2.7 74.0 2.2 75.0 2.3 76.0 2.7 77.0 16.9 78.0 5.5 91.0 1.7 102.0 4.4 103.0 15.9 104.0 1.5 105.0 5.4 115.0 2.2 117.0 1.1 126.0 1.0 127.0 3.8 128.0 6.5 129.0 3.2 131.0 100.0 132.0 9.9 145.0 4.3 146.0 2.6
90 MHz in CDCl3
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1H NMR 89.56 MHz C10 H10 O 0.034 g : 0.5 ml CDCl3 2-phenyl-3-butyn-2-ol 
Assign. Shift(ppm)
A 7.64 B 7.35 C 7.31 D 2.66 E 2.531 F 1.775 CONFIRMED BY LAOCN PROGRAM J(E,F)=0.3HZ
Hz ppm Int.692.63 7.734 31 690.56 7.711 133 689.81 7.703 71 689.31 7.697 62 688.38 7.687 86 687.75 7.680 92 686.63 7.667 93 685.94 7.660 116 685.25 7.652 89 684.31 7.641 78 682.44 7.620 220 680.69 7.601 222 678.44 7.576 35 677.44 7.565 43 669.56 7.477 36 668.75 7.468 30 665.44 7.431 45 664.63 7.422 84 662.94 7.403 65 660.81 7.379 193 660.19 7.372 205 658.13 7.349 201 654.94 7.313 290 653.13 7.293 342 651.56 7.276 76 650.63 7.265 60 649.69 7.255 47 648.88 7.246 51 648.50 7.241 51 237.88 2.657 638 226.75 2.532 289 159.19 1.778 1000
in CDCl3
KBr disc
nujol mull
4880 A,200 M,powder
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