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MassMS-IW-4044 (-)-1,6-bis(o-chlorophenyl)-1,6-diphenyl-2,4-hexadiyne-1,6-diol C30H20Cl2O2 (Mass of molecular ion: 482)
Source Temperature: 180 °C Sample Temperature: 170 °C Direct, 75 eV
17.0 1.2 18.0 6.8 28.0 1.0 39.0 1.2 49.0 1.4 50.0 7.2 51.0 12.0 52.0 1.0 63.0 2.1 74.0 2.5 75.0 11.1 76.0 7.4 77.0 49.5 78.0 4.4 86.0 1.0 87.0 1.8 88.0 3.6 93.5 1.0 94.0 1.6 99.0 1.5 100.0 3.3 100.5 1.7 101.0 9.4 101.5 2.1 105.0 100.0 105.5 1.1 106.0 8.9 106.5 2.2 107.0 1.2 111.0 17.9 112.0 2.0 113.0 6.1 125.0 2.0 126.0 4.7 127.0 2.3 137.0 1.7 138.0 1.1 139.0 54.9 140.0 4.3 141.0 18.1 142.0 1.4 150.0 1.5 151.0 2.6 152.0 4.6 153.0 2.2 154.0 4.8 155.0 3.4 160.0 1.9 162.0 1.0 163.0 1.3 165.0 1.1 176.0 1.2 180.0 1.0 181.0 4.7 187.0 1.4 188.0 6.2 189.0 3.1 190.0 2.1 191.0 1.0 199.0 1.2 200.0 4.4 201.0 6.5 202.0 36.5 203.0 23.7 204.0 3.6 211.0 2.1 212.0 1.7 213.0 6.3 214.0 1.7 215.0 1.4 216.0 42.0 217.0 6.5 218.0 14.1 219.0 2.1 229.0 1.0 230.0 4.2 231.0 43.9 232.0 8.2 238.0 1.6 249.0 2.1 265.0 5.4 266.0 1.4 267.0 1.9 289.0 1.2 307.0 1.0 343.0 2.9 345.0 1.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C30 H20 Cl2 O2 0.038 g : 0.5 ml CDCl3 (-)-1,6-bis(o-chlorophenyl)-1,6-diphenyl-2,4-hexadiyne-1,6-diol 
Assign. Shift(ppm)
A 7.885 B 7.473 C 7.48 to 7.46 D 7.272 E 3.26
Hz ppm Int.3156.13 7.898 214 3154.66 7.894 181 3151.25 7.886 65 3149.90 7.882 67 3148.80 7.879 203 3148.32 7.878 225 3146.48 7.874 202 2993.04 7.490 60 2991.70 7.486 319 2990.48 7.483 136 2989.50 7.481 216 2987.55 7.476 140 2986.45 7.473 147 2985.47 7.471 201 2983.64 7.466 446 2982.06 7.462 411 2979.98 7.457 44 2978.88 7.454 50 2937.62 7.351 78 2935.91 7.347 59 2933.59 7.341 210 2931.76 7.336 216 2930.79 7.334 201 2929.20 7.330 449 2926.76 7.324 295 2925.05 7.320 530 2922.97 7.314 712 2922.49 7.313 709 2921.26 7.310 756 2918.21 7.302 391 2916.38 7.298 166 2912.11 7.287 273 2910.28 7.283 300 2907.84 7.276 78 2905.40 7.270 141 2903.93 7.267 119 2902.95 7.264 198 2897.22 7.250 83 2895.51 7.246 73 1302.73 3.260 1000
KBr disc
nujol mull
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