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MassMS-IW-8155 diphenylsilane C12H12Si (Mass of molecular ion: 184)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
29.0 1.0 50.0 1.1 51.0 2.5 53.0 10.9 54.0 2.0 55.0 2.1 66.0 1.0 67.0 1.0 77.0 3.0 78.0 2.5 79.0 7.9 80.0 2.1 81.0 2.4 91.0 2.8 103.0 4.2 104.0 1.4 105.0 59.8 106.0 100.0 107.0 16.8 108.0 4.4 129.0 2.1 131.0 1.3 152.0 1.0 153.0 1.3 154.0 1.3 155.0 3.9 179.0 1.1 180.0 4.3 181.0 14.4 182.0 5.4 183.0 22.8 184.0 62.6 185.0 11.7 186.0 3.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C12 H12 Si 0.05 ml : 0.5 ml CDCl3 diphenylsilane 
Assign. Shift(ppm)
A 7.578 B 7.362 C 7.329 D 4.932
Hz ppm Int.3036.50 7.598 52 3035.40 7.596 112 3033.57 7.591 534 3031.98 7.587 608 3030.52 7.583 293 3028.81 7.579 99 3027.83 7.577 234 3026.86 7.574 257 3025.88 7.572 641 3024.05 7.567 634 3021.12 7.560 54 2954.47 7.393 51 2952.88 7.389 101 2951.29 7.385 68 2949.34 7.380 77 2945.43 7.371 327 2942.63 7.364 130 2940.31 7.358 289 2938.60 7.353 452 2936.77 7.349 254 2936.04 7.347 188 2934.94 7.344 470 2934.20 7.342 545 2932.74 7.339 347 2928.47 7.328 342 2927.12 7.325 576 2926.51 7.323 457 2922.00 7.312 116 2920.65 7.309 227 2919.92 7.307 154 2918.46 7.303 185 2070.80 5.182 35 1971.19 4.933 1000 1871.46 4.683 35
in CDCl3
liquid film
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