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MassMS2014-05092CW iodomethane CH3I (Mass of molecular ion: 142)
Source Temperature: 250 °C Sample Temperature: 250 °C Reservoir, 70 eV
15.0 4.3 28.0 4.7 32.0 1.2 94.0 1.2 96.0 1.2 127.0 26.8 128.0 1.7 139.0 4.1 140.0 3.6 141.0 13.1 142.0 100.0 143.0 1.1
parameter in CCl4
in CDCl3
parameter in CDCl3
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1H NMR 300 MHz C H3 I 10 wt% in CCl4 iodomethane 
Parameter ppm Hz
D(A) 2.162 LACEY,M.J. ET AL. AUST.J.CHEM. 23, 1421 (1970) J(GEM):-9.355HZ DETERMINED IN NEAT LIQUID. J(C-13,H):151.0HZ.
Hz ppm Int.648.60 2.162 1000
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1H NMR 300 MHz C H3 I 0.05 ml : 0.5 ml CDCl3 iodomethane Parameter ppm Hz
D(A) 2.165
Hz ppm Int.649.50 2.165 1000
in CDCl3
liquid film
PHOTOLYSIS, ON SILICA GEL
CH3 RADICAL, PHOTOLYSIS OF 13CH3I(50%)-VYCOR GLASS
METHYL RADICAL, PHOTOLYSIS, ON SILICA GEL
IO RADICAL, REACTION OF O ATOM
CH3 RADICAL, PHOTOLYSIS, ON VYCOR GLASS
METHYL RADICAL, X-IRRAD.(53%13C), 77K
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