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MassMS-NW-0072 methanol CH4O (Mass of molecular ion: 32)
Source Temperature: 220 °C Sample Temperature: 25 °C Reservoir, 75 eV
14.0 1.7 15.0 12.4 28.0 4.6 29.0 44.6 30.0 6.5 31.0 100.0 32.0 74.4 33.0 1.2
in CD3CN
90 MHz in CDCl3
in DMSO-d6
in CDCl3
parameter in CDCl3
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1H NMR 89.56 MHz C H4 O 0.05 ml : 0.5 ml CDCl3 methanol 
Assign. Shift(ppm)
A 3.66 B 3.43 J(A,B)=4.6HZ.
Hz ppm Int.336.81 3.761 36 331.25 3.699 135 326.13 3.642 188 321.75 3.593 124 308.63 3.447 1000 304.00 3.395 562
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1H NMR 300 MHz C H4 O 0.1 ml : 0.5 ml CDCl3 methanol Parameter ppm Hz
D(A) 4.19 D(B) 3.410
Hz ppm Int.1257.00 4.190 208 1023.00 3.410 1000
in DMSO-d6
in CD3CN
in CDCl3
in CD3OD
liquid film
4880 A,200 M,liquid
REDUCTION WITH TICL3 AND H2O2
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