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N-(2-氯乙基)吡咯烷盐酸盐

产品名称 N-(2-氯乙基)吡咯烷盐酸盐

CAS号7250-67-1

分子式C6H13Cl2N

分子量170.08

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  • Mass

    MS-NW-7034          
    N-(2-chloroethyl)pyrrolidine hydrochloride
    C6H12ClN HCl        (Mass of molecular ion:    133)
    

       Source Temperature: 180 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          15.0       3.5
          26.0       1.4
          27.0      10.8
          28.0       7.8
          29.0       3.0
          30.0       4.3
          35.0       3.1
          36.0      20.1
          37.0       1.0
          38.0       6.9
          39.0       4.4
          40.0       1.1
          41.0       8.0
          42.0      27.3
          43.0       9.9
          54.0       2.2
          55.0      11.1
          56.0       6.0
          63.0       3.4
          65.0       1.1
          68.0       1.1
          69.0       1.0
          70.0       3.0
          82.0       1.1
          84.0     100.0
          85.0       5.7
          90.0       1.2
          96.0       1.3
          98.0       1.6
         132.0       3.4
         133.0       4.9
         134.0       1.5
         135.0       1.6
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6 H12 Cl N 0.036 g : 0.5 ml CDCl3
    N-(2-chloroethyl)pyrrolidine hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 12.3 B 4.060 C *1 3.83 D 3.59 E *1 3.12 F 2.177 ASSIGNED BY C-H COSY.

         Hz     ppm     Int.
    

       4903.37  12.270     39
       1629.27   4.077    453
       1622.67   4.061   1000
       1616.08   4.044    513
       1545.01   3.866     37
       1533.29   3.837    114
       1532.55   3.835    114
       1528.89   3.826    124
       1528.34   3.825    124
       1527.97   3.824    124
       1525.04   3.816    112
       1441.89   3.608    108
       1436.03   3.594    206
       1432.18   3.584    201
       1426.32   3.569     93
       1244.98   3.116    115
       1244.62   3.115    115
        872.06   2.183    359
        868.39   2.173    336
        857.22   2.145     66
    

in CDCl3



KBr disc



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