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网站主页CAS数据库列表 56824-22-7更多图谱N-(2-氯乙基)-吡咯烷盐酸盐(56824-22-7)红外图谱(IR1)

N-(2-氯乙基)-吡咯烷盐酸盐

产品名称 N-(2-氯乙基)-吡咯烷盐酸盐

CAS号56824-22-7

分子式C7H15Cl2N

分子量184.1


  • Mass

    MS-IW-0699          
    2-(2-chloroethyl)-1-methylpyrrolidine hydrochloride
    C7H14ClN HCl        (Mass of molecular ion:    147)
    

       Source Temperature: 150 °C
       Sample Temperature: 110 °C
       Direct, 75 eV
    

          27.0       1.0
          28.0       1.0
          36.0      15.5
          38.0       5.1
          41.0       2.1
          42.0      10.2
          55.0       1.4
          70.0       2.3
          82.0       4.6
          84.0     100.0
          85.0       6.0
         146.0       1.4
         147.0       4.2
         149.0       1.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H14 Cl N 0.040 g : 0.5 ml CDCl3
    2-(2-chloroethyl)-1-methylpyrrolidine hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 12.1 B 3.86 C 3.598 D 3.462 E 3.018 F 2.899 G 2.49 J 2.392 K 2.24 L 2.14 M 1.973 ASSIGNED BY H-H AND C-H COSY.

         Hz     ppm     Int.
    

       4839.44  12.110     35
       1558.93   3.901     35
       1553.98   3.889    129
       1550.69   3.881     54
       1548.67   3.876    197
       1545.38   3.867     83
       1542.45   3.860    181
       1539.88   3.854     85
       1537.13   3.847    237
       1534.20   3.839     78
       1532.00   3.834    108
       1528.71   3.826     39
       1450.31   3.629    106
       1445.00   3.616    111
       1441.89   3.608     87
       1441.52   3.607     87
       1438.77   3.601     94
       1436.39   3.595    117
       1433.46   3.587     92
       1430.35   3.580     72
       1429.80   3.578     69
       1424.85   3.566     87
       1395.55   3.492     41
       1388.04   3.474     66
       1379.98   3.453     68
       1372.47   3.435     44
       1223.92   3.063     37
       1216.41   3.044     71
       1215.13   3.041     59
       1212.56   3.035     42
       1207.62   3.022     82
       1205.05   3.016     74
       1203.77   3.013     55
       1200.11   3.003     47
       1197.54   2.997     53
       1196.26   2.994     70
       1188.75   2.975     38
       1161.09   2.906   1000
       1156.15   2.893    987
       1007.78   2.522     86
       1004.12   2.513     94
       1002.47   2.509    160
        998.99   2.500    170
        993.86   2.487    182
        989.83   2.477    149
        988.73   2.474     99
        984.52   2.464     84
        972.61   2.434     33
        968.22   2.423     35
        964.55   2.414     51
        959.98   2.403     81
        957.04   2.395     47
        955.40   2.391     49
        952.28   2.383     81
        947.15   2.370     57
        944.04   2.363     40
        939.46   2.351     43
        911.80   2.282     30
        906.49   2.269     45
        902.46   2.259     48
        898.43   2.249     76
        894.22   2.238     56
        892.94   2.235     40
        889.46   2.226     67
        884.88   2.215     51
        881.40   2.206     32
        873.52   2.186     33
        868.21   2.173     31
        864.91   2.165     52
        859.97   2.152     62
        857.22   2.145     59
        852.09   2.133     74
        848.61   2.124     38
        847.69   2.122     34
        846.60   2.119     31
        843.66   2.111     53
        838.72   2.099     31
        807.21   2.020     51
        799.70   2.002     48
        797.69   1.996     87
        794.21   1.988     48
        790.18   1.978     71
        788.17   1.973     55
        786.70   1.969     53
        784.69   1.964     75
        780.66   1.954     37
        777.18   1.945     62
        775.34   1.941     41
    

in CDCl3



KBr disc



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