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MassMS-IW-0699 2-(2-chloroethyl)-1-methylpyrrolidine hydrochloride C7H14ClN HCl (Mass of molecular ion: 147)
Source Temperature: 150 °C Sample Temperature: 110 °C Direct, 75 eV
27.0 1.0 28.0 1.0 36.0 15.5 38.0 5.1 41.0 2.1 42.0 10.2 55.0 1.4 70.0 2.3 82.0 4.6 84.0 100.0 85.0 6.0 146.0 1.4 147.0 4.2 149.0 1.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H14 Cl N 0.040 g : 0.5 ml CDCl3 2-(2-chloroethyl)-1-methylpyrrolidine hydrochloride 
Assign. Shift(ppm)
A 12.1 B 3.86 C 3.598 D 3.462 E 3.018 F 2.899 G 2.49 J 2.392 K 2.24 L 2.14 M 1.973 ASSIGNED BY H-H AND C-H COSY.
Hz ppm Int.4839.44 12.110 35 1558.93 3.901 35 1553.98 3.889 129 1550.69 3.881 54 1548.67 3.876 197 1545.38 3.867 83 1542.45 3.860 181 1539.88 3.854 85 1537.13 3.847 237 1534.20 3.839 78 1532.00 3.834 108 1528.71 3.826 39 1450.31 3.629 106 1445.00 3.616 111 1441.89 3.608 87 1441.52 3.607 87 1438.77 3.601 94 1436.39 3.595 117 1433.46 3.587 92 1430.35 3.580 72 1429.80 3.578 69 1424.85 3.566 87 1395.55 3.492 41 1388.04 3.474 66 1379.98 3.453 68 1372.47 3.435 44 1223.92 3.063 37 1216.41 3.044 71 1215.13 3.041 59 1212.56 3.035 42 1207.62 3.022 82 1205.05 3.016 74 1203.77 3.013 55 1200.11 3.003 47 1197.54 2.997 53 1196.26 2.994 70 1188.75 2.975 38 1161.09 2.906 1000 1156.15 2.893 987 1007.78 2.522 86 1004.12 2.513 94 1002.47 2.509 160 998.99 2.500 170 993.86 2.487 182 989.83 2.477 149 988.73 2.474 99 984.52 2.464 84 972.61 2.434 33 968.22 2.423 35 964.55 2.414 51 959.98 2.403 81 957.04 2.395 47 955.40 2.391 49 952.28 2.383 81 947.15 2.370 57 944.04 2.363 40 939.46 2.351 43 911.80 2.282 30 906.49 2.269 45 902.46 2.259 48 898.43 2.249 76 894.22 2.238 56 892.94 2.235 40 889.46 2.226 67 884.88 2.215 51 881.40 2.206 32 873.52 2.186 33 868.21 2.173 31 864.91 2.165 52 859.97 2.152 62 857.22 2.145 59 852.09 2.133 74 848.61 2.124 38 847.69 2.122 34 846.60 2.119 31 843.66 2.111 53 838.72 2.099 31 807.21 2.020 51 799.70 2.002 48 797.69 1.996 87 794.21 1.988 48 790.18 1.978 71 788.17 1.973 55 786.70 1.969 53 784.69 1.964 75 780.66 1.954 37 777.18 1.945 62 775.34 1.941 41
in CDCl3
KBr disc
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