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MS-NW-6227 4-bromo-m-toluidine C7H8BrN (Mass of molecular ion: 185)
Source Temperature: 250 °C Sample Temperature: 190 °C Reservoir, 75 eV
27.0 2.4 28.0 5.0 30.0 2.4 37.0 1.8 38.0 3.4 39.0 6.4 40.0 1.5 41.0 3.0 42.0 1.5 50.0 4.6 51.0 9.4 51.5 2.1 52.0 8.1 52.5 8.1 53.0 9.6 54.0 2.4 61.0 1.3 62.0 2.7 63.0 4.9 64.0 1.6 65.0 2.6 66.0 1.9 74.0 1.7 75.0 1.6 76.0 1.9 77.0 21.0 78.0 12.7 79.0 17.4 80.0 3.0 89.0 2.5 91.0 1.0 92.5 2.7 93.5 2.6 104.0 14.3 105.0 9.8 106.0 58.7 107.0 5.0 184.0 7.7 185.0 100.0 186.0 15.4 187.0 96.9 188.0 8.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H8 Br N 0.050 g : 0.5 ml CDCl3 4-bromo-m-toluidine Assign. Shift(ppm)
A 7.237 B 6.549 C 6.376 D 3.51 E 2.283
Hz ppm Int.
652.75 7.289 178 644.38 7.195 219 588.19 6.568 115 585.50 6.538 162 576.06 6.433 106 573.25 6.401 74 567.69 6.339 83 564.81 6.307 63 314.69 3.514 87 204.63 2.285 1000
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