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MassMS-NW-2181 m-toluidine C7H9N (Mass of molecular ion: 107)
Source Temperature: 270 °C Sample Temperature: 170 °C Reservoir, 75 eV
27.0 2.6 28.0 3.9 30.0 1.4 38.0 2.2 39.0 7.3 40.0 1.3 41.0 2.6 42.0 2.1 50.0 2.3 51.0 4.6 52.0 4.1 52.5 1.3 53.0 5.3 53.5 2.3 54.0 2.0 62.0 1.0 63.0 2.5 64.0 1.3 65.0 4.1 66.0 1.7 77.0 12.2 78.0 4.4 79.0 13.7 80.0 5.1 89.0 2.7 90.0 2.8 91.0 3.6 104.0 2.2 105.0 1.0 106.0 81.1 107.0 100.0 108.0 7.8
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H9 N 0.04 ml : 0.5 ml CDCl3 m-toluidine 
Assign. Shift(ppm)
A 7.01 B 6.56 C 6.49 D 6.47 E 3.46 F 2.25
Hz ppm Int.637.38 7.117 76 629.94 7.034 125 628.75 7.021 107 626.88 7.000 39 621.44 6.939 159 592.88 6.620 54 592.19 6.613 92 591.56 6.606 131 590.88 6.598 138 590.25 6.591 119 589.56 6.583 84 583.88 6.520 113 582.06 6.500 273 581.50 6.493 309 580.81 6.486 288 580.19 6.479 252 579.50 6.471 210 578.81 6.463 150 577.88 6.453 95 577.19 6.445 77 575.75 6.429 86 575.19 6.423 99 574.63 6.417 91 574.06 6.410 77 573.50 6.404 56 572.81 6.396 45 572.25 6.390 40 310.19 3.464 810 201.06 2.245 1000
in CDCl3
CCl4 solution
liquid film
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