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MS-IW-0240 2-chloro-6-nitrobenzaldehyde C7H4ClNO3 (Mass of molecular ion: 185)
Source Temperature: 260 °C Sample Temperature: 160 °C Reservoir, 75 eV
18.0 1.8 28.0 2.7 29.0 2.8 30.0 5.1 36.0 1.0 37.0 2.7 38.0 2.1 39.0 3.2 44.0 1.1 49.0 2.1 50.0 11.8 51.0 6.6 61.0 2.9 62.0 2.7 63.0 10.6 64.0 1.9 73.0 12.9 74.0 15.8 75.0 72.7 76.0 9.7 77.0 1.4 78.0 2.7 84.0 4.3 85.0 5.0 86.0 2.3 87.0 2.4 90.0 1.3 91.0 28.7 92.0 4.8 99.0 79.3 100.0 4.7 101.0 25.7 102.0 1.5 109.0 1.1 110.0 27.5 111.0 10.5 112.0 9.6 113.0 3.7 126.0 2.6 127.0 4.5 128.0 1.1 129.0 1.4 138.0 25.6 139.0 2.4 140.0 8.2 155.0 100.0 156.0 8.0 157.0 32.3 158.0 2.5 168.0 2.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H4 Cl N O3 0.038 g : 0.5 ml CDCl3 2-chloro-6-nitrobenzaldehyde Assign. Shift(ppm)
A 10.376 B 7.977 C 7.771 D 7.642
Hz ppm Int.
4147.03 10.377 1000 3192.75 7.989 280 3191.99 7.987 281 3184.51 7.969 314 3183.90 7.967 308 3111.11 7.785 300 3110.05 7.782 294 3106.84 7.774 33 3105.77 7.772 36 3103.03 7.765 412 3101.96 7.762 378 3061.52 7.661 405 3053.44 7.641 631 3047.64 7.626 26 3045.20 7.620 267
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