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MS-NW-3550 2-chloro-5-nitrobenzaldehyde C7H4ClNO3 (Mass of molecular ion: 185)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
28.0 3.9 29.0 6.5 30.0 9.5 36.0 1.4 37.0 4.5 38.0 3.3 39.0 1.7 49.0 2.6 50.0 16.8 51.0 7.7 53.0 1.1 61.0 3.7 62.0 3.3 63.0 5.5 64.0 1.1 72.0 1.0 73.0 6.5 74.0 23.6 75.0 100.0 76.0 11.5 84.0 3.6 85.0 6.2 86.0 1.9 87.0 2.5 99.0 10.4 101.0 3.8 103.0 4.2 109.0 2.1 110.0 11.5 111.0 25.2 112.0 5.4 113.0 8.4 126.0 2.2 127.0 2.0 138.0 15.7 139.0 23.6 140.0 7.0 141.0 7.9 149.0 1.3 155.0 5.2 157.0 2.1 169.0 1.8 184.0 75.1 185.0 75.9 186.0 30.8 187.0 25.9 188.0 2.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H4 Cl N O3 0.043 g : 0.5 ml CDCl3 2-chloro-5-nitrobenzaldehyde Assign. Shift(ppm)
A 10.497 B 8.736 C 8.387 D 7.709 J(B,C)=2.8HZ. J(C,D)=8.8HZ.
Hz ppm Int.
940.21 10.499 1000 784.20 8.757 263 781.35 8.725 312 757.62 8.460 204 754.83 8.429 166 748.83 8.362 260 746.04 8.331 229 694.34 7.753 351 685.55 7.655 270
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