2-氯-3-吗啉-1,4-萘醌

Mass

MS-NW-7905          
2-chloro-3-morpholino-1,4-naphthoquinone
C14H12ClNO3         (Mass of molecular ion:    277)

   Source Temperature: 180 °C
   Sample Temperature: 130 °C
   Direct, 75 eV

      15.0       2.6
      18.0       4.0
      26.0       1.8
      27.0       7.1
      28.0       9.1
      29.0       3.1
      30.0       2.0
      31.0       2.0
      36.0       1.8
      38.0       1.0
      39.0       4.2
      41.0       2.8
      42.0      17.1
      43.0       2.9
      44.0       1.2
      45.0       6.6
      50.0       9.7
      51.0       6.0
      52.0       3.9
      53.0       1.7
      54.0       2.5
      55.0       3.0
      56.0      10.6
      57.0       3.4
      58.0       1.2
      59.0       1.0
      61.0       1.0
      62.0       2.2
      63.0       2.7
      64.0       2.1
      66.0       1.4
      68.0       2.3
      69.0       1.0
      70.0       1.5
      72.0       7.6
      73.0       1.3
      74.0       6.4
      75.0      10.6
      76.0      19.2
      77.0       8.2
      77.5       1.1
      78.0       1.8
      80.0       2.8
      85.0       1.6
      86.0       5.1
      87.0       6.4
      88.0       3.0
      89.0       3.2
      94.0       1.2
      95.5       1.9
      98.0       1.4
      99.0       8.5
     100.0       3.5
     101.0      13.8
     102.0       5.1
     103.0       1.6
     104.0       7.0
     105.0       6.2
     109.0       1.7
     109.5       2.9
     110.0       1.0
     110.5       1.1
     111.0       1.5
     113.0       1.6
     114.0       5.7
     115.0       3.6
     116.0       1.3
     116.5       1.3
     123.0       2.3
     123.5       5.2
     124.0       1.3
     124.5       1.8
     125.0       1.1
     126.0       5.2
     127.0       3.6
     128.0       6.1
     129.0      20.4
     130.0       4.3
     135.0       8.4
     136.0       4.3
     137.0       3.4
     138.0       1.8
     140.0       1.0
     143.0       1.9
     149.0       1.4
     151.0       1.1
     154.0      12.4
     155.0       2.7
     156.0       4.0
     157.0      81.5
     158.0      10.5
     159.0       1.9
     163.0       6.0
     164.0       2.3
     165.0       2.8
     166.0       1.0
     167.0       1.1
     171.0       4.2
     172.0       3.7
     173.0       1.6
     177.0       2.2
     179.0       1.0
     182.0       1.0
     183.0       2.8
     184.0       5.3
     185.0       3.7
     186.0       3.7
     191.0       4.8
     192.0      16.8
     193.0       4.8
     194.0       6.2
     195.0       1.5
     196.0       1.1
     198.0       7.0
     199.0       2.0
     200.0       1.1
     205.0       2.2
     206.0      17.1
     207.0       6.8
     208.0       6.6
     209.0       2.7
     210.0       2.8
     211.0       3.5
     212.0       9.1
     213.0       3.6
     214.0       4.5
     216.0       1.5
     218.0       6.8
     219.0       9.0
     220.0      97.1
     221.0      15.7
     222.0      32.6
     223.0       5.0
     224.0       5.7
     225.0       1.1
     226.0       1.1
     233.0      12.8
     234.0       8.4
     235.0       5.5
     236.0       2.8
     241.0       3.4
     242.0      32.8
     243.0       6.3
     244.0       1.1
     246.0      17.0
     247.0       2.9
     248.0       6.8
     249.0       1.3
     276.0       1.9
     277.0     100.0
     278.0      16.9
     279.0      35.0
     280.0       5.7
     281.0       1.1

Assign. Shift(ppm) A 8.096 B 7.997 C *1 7.71 D *1 7.67 E 3.870 F 3.630

     Hz     ppm     Int.

   3240.48   8.109    265
   3239.01   8.105    333
   3233.76   8.092    239
   3232.91   8.090    269
   3231.81   8.087    293
   3231.45   8.086    280
   3200.68   8.009    251
   3200.32   8.008    258
   3199.10   8.005    243
   3198.36   8.003    224
   3193.12   7.990    358
   3191.65   7.987    297
   3088.99   7.730    115
   3087.40   7.726    144
   3085.33   7.721     36
   3081.54   7.711    329
   3079.96   7.707    348
   3074.34   7.693    340
   3072.75   7.689    431
   3071.04   7.685    348
   3065.43   7.671    344
   3063.84   7.667    306
   3060.42   7.658     33
   3057.98   7.652    126
   3056.52   7.648    105
   1551.51   3.883    822
   1547.00   3.871   1000
   1542.24   3.859    952
   1532.96   3.836     35
   1532.59   3.835     35
   1464.72   3.666     38
   1455.08   3.641    962
   1450.32   3.629    990
   1445.80   3.618    793
   1436.16   3.594     32