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MassMS-NW-7905 2-chloro-3-morpholino-1,4-naphthoquinone C14H12ClNO3 (Mass of molecular ion: 277)
Source Temperature: 180 °C Sample Temperature: 130 °C Direct, 75 eV
15.0 2.6 18.0 4.0 26.0 1.8 27.0 7.1 28.0 9.1 29.0 3.1 30.0 2.0 31.0 2.0 36.0 1.8 38.0 1.0 39.0 4.2 41.0 2.8 42.0 17.1 43.0 2.9 44.0 1.2 45.0 6.6 50.0 9.7 51.0 6.0 52.0 3.9 53.0 1.7 54.0 2.5 55.0 3.0 56.0 10.6 57.0 3.4 58.0 1.2 59.0 1.0 61.0 1.0 62.0 2.2 63.0 2.7 64.0 2.1 66.0 1.4 68.0 2.3 69.0 1.0 70.0 1.5 72.0 7.6 73.0 1.3 74.0 6.4 75.0 10.6 76.0 19.2 77.0 8.2 77.5 1.1 78.0 1.8 80.0 2.8 85.0 1.6 86.0 5.1 87.0 6.4 88.0 3.0 89.0 3.2 94.0 1.2 95.5 1.9 98.0 1.4 99.0 8.5 100.0 3.5 101.0 13.8 102.0 5.1 103.0 1.6 104.0 7.0 105.0 6.2 109.0 1.7 109.5 2.9 110.0 1.0 110.5 1.1 111.0 1.5 113.0 1.6 114.0 5.7 115.0 3.6 116.0 1.3 116.5 1.3 123.0 2.3 123.5 5.2 124.0 1.3 124.5 1.8 125.0 1.1 126.0 5.2 127.0 3.6 128.0 6.1 129.0 20.4 130.0 4.3 135.0 8.4 136.0 4.3 137.0 3.4 138.0 1.8 140.0 1.0 143.0 1.9 149.0 1.4 151.0 1.1 154.0 12.4 155.0 2.7 156.0 4.0 157.0 81.5 158.0 10.5 159.0 1.9 163.0 6.0 164.0 2.3 165.0 2.8 166.0 1.0 167.0 1.1 171.0 4.2 172.0 3.7 173.0 1.6 177.0 2.2 179.0 1.0 182.0 1.0 183.0 2.8 184.0 5.3 185.0 3.7 186.0 3.7 191.0 4.8 192.0 16.8 193.0 4.8 194.0 6.2 195.0 1.5 196.0 1.1 198.0 7.0 199.0 2.0 200.0 1.1 205.0 2.2 206.0 17.1 207.0 6.8 208.0 6.6 209.0 2.7 210.0 2.8 211.0 3.5 212.0 9.1 213.0 3.6 214.0 4.5 216.0 1.5 218.0 6.8 219.0 9.0 220.0 97.1 221.0 15.7 222.0 32.6 223.0 5.0 224.0 5.7 225.0 1.1 226.0 1.1 233.0 12.8 234.0 8.4 235.0 5.5 236.0 2.8 241.0 3.4 242.0 32.8 243.0 6.3 244.0 1.1 246.0 17.0 247.0 2.9 248.0 6.8 249.0 1.3 276.0 1.9 277.0 100.0 278.0 16.9 279.0 35.0 280.0 5.7 281.0 1.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C14 H12 Cl N O3 0.040 g : 0.5 ml CDCl3 2-chloro-3-morpholino-1,4-naphthoquinone 
Assign. Shift(ppm)
A 8.096 B 7.997 C *1 7.71 D *1 7.67 E 3.870 F 3.630
Hz ppm Int.3240.48 8.109 265 3239.01 8.105 333 3233.76 8.092 239 3232.91 8.090 269 3231.81 8.087 293 3231.45 8.086 280 3200.68 8.009 251 3200.32 8.008 258 3199.10 8.005 243 3198.36 8.003 224 3193.12 7.990 358 3191.65 7.987 297 3088.99 7.730 115 3087.40 7.726 144 3085.33 7.721 36 3081.54 7.711 329 3079.96 7.707 348 3074.34 7.693 340 3072.75 7.689 431 3071.04 7.685 348 3065.43 7.671 344 3063.84 7.667 306 3060.42 7.658 33 3057.98 7.652 126 3056.52 7.648 105 1551.51 3.883 822 1547.00 3.871 1000 1542.24 3.859 952 1532.96 3.836 35 1532.59 3.835 35 1464.72 3.666 38 1455.08 3.641 962 1450.32 3.629 990 1445.80 3.618 793 1436.16 3.594 32
in CDCl3
KBr disc
nujol mull
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