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2,3-二氯苯胺

产品名称 2,3-二氯苯胺

CAS号608-27-5

分子式C6H5Cl2N

分子量162.02

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  • Mass

    MS-NW-0840          
    2,3-dichloroaniline
    C6H5Cl2N            (Mass of molecular ion:    161)
    

       Source Temperature: 280 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          28.0       4.7
          36.0       1.0
          37.0       3.6
          38.0       3.7
          39.0       3.9
          41.0       2.7
          42.0       1.2
          43.0       1.0
          44.5       5.0
          45.0       1.1
          45.5       1.5
          49.0       1.2
          50.0       1.5
          51.0       1.1
          52.0       3.8
          57.0       1.1
          61.0       3.4
          62.0       6.1
          62.5       6.3
          63.0      14.0
          63.5       2.1
          64.0       4.1
          65.0       3.5
          72.0       2.0
          73.0       4.6
          74.0       1.8
          75.0       1.9
          80.5       6.0
          81.5       3.7
          86.0       1.5
          88.0       1.2
          89.0       3.4
          90.0      26.1
          91.0       5.0
          97.0       2.0
          98.0       2.8
          99.0      12.5
         100.0       2.1
         101.0       4.2
         124.0       1.4
         125.0       7.4
         126.0      11.5
         127.0       3.4
         128.0       3.7
         133.0       3.9
         134.0       2.9
         135.0       2.9
         136.0       1.9
         160.0       1.0
         161.0     100.0
         162.0       7.8
         163.0      63.9
         164.0       4.5
         165.0      10.4
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H5 Cl2 N 0.04 ml : 0.5 ml CDCl3
    2,3-dichloroaniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.936 B 6.827 C 6.626 D 4.1

         Hz     ppm     Int.
    

        631.63   7.053    219
        624.19   6.970    364
        623.69   6.964    599
        616.31   6.882   1000
        614.44   6.861    609
        612.25   6.837    914
        606.50   6.772    321
        604.31   6.748    147
        597.13   6.668    684
        594.94   6.643    485
        589.75   6.585    399
        587.56   6.561    355
        369.06   4.121     83
    

in CDCl3



liquid film





OXIDATION WITH PERBENZOIC ACID