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网站主页CAS数据库列表 108-42-9更多图谱间氯苯胺(108-42-9)质谱(MS)

间氯苯胺

产品名称 间氯苯胺

CAS号108-42-9

分子式C6H6ClN

分子量127.57

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  • Mass

    MS-NW-8468          
    m-chloroaniline
    C6H6ClN             (Mass of molecular ion:    127)
    

       Source Temperature: 250 °C
       Sample Temperature: 140 °C
       Reservoir, 75 eV
    

          28.0       3.5
          37.0       2.2
          38.0       4.2
          39.0       9.0
          40.0       1.3
          41.0       3.9
          42.0       1.4
          44.5       1.3
          45.5       5.0
          50.0       2.1
          51.0       1.8
          52.0       4.1
          61.0       2.0
          62.0       3.3
          63.0       7.5
          63.5       2.7
          64.0       7.2
          65.0      30.5
          66.0       3.9
          73.0       2.8
          74.0       1.3
          75.0       2.3
          90.0       2.3
          91.0       6.9
          92.0      21.9
          93.0       1.8
          99.0       4.8
         100.0       9.9
         101.0       2.4
         102.0       3.2
         126.0       1.6
         127.0     100.0
         128.0       7.5
         129.0      31.9
         130.0       2.2
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6 H6 Cl N 0.05 ml : 0.5 ml CDCl3
    m-chloroaniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.003 B 6.686 C 6.589 D 6.463 E 3.66

         Hz     ppm     Int.
    

       2809.08   7.029    514
       2800.90   7.009   1000
       2793.09   6.989    611
       2677.61   6.700    450
       2676.76   6.698    479
       2675.66   6.696    504
       2674.68   6.693    488
       2669.68   6.681    405
       2668.82   6.678    424
       2667.72   6.676    468
       2666.87   6.674    447
       2635.50   6.595    598
       2633.30   6.590    999
       2631.23   6.584    596
       2588.38   6.477    473
       2587.40   6.475    472
       2586.06   6.471    441
       2585.21   6.469    446
       2583.37   6.465     42
       2582.28   6.462     44
       2580.32   6.457    447
       2579.35   6.455    451
       2578.00   6.451    427
       2577.15   6.449    424
       1462.16   3.659    176
          0.00   0.001    336
    

in CDCl3



CCl4 solution



liquid film





OXIDATION WITH PERBENZOIC ACID