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网站主页CAS数据库列表 606-22-4更多图谱2,6-二硝基苯胺(606-22-4)核磁图(13CNMR)

2,6-二硝基苯胺

产品名称 2,6-二硝基苯胺

CAS号606-22-4

分子式C6H5N3O4

分子量183.12

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  • Mass

    MS-NW-6469          
    2,6-dinitroaniline
    C6H5N3O4            (Mass of molecular ion:    183)
    

       Source Temperature: 280 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          18.0       3.4
          26.0       1.1
          27.0       2.5
          28.0       5.1
          30.0       8.5
          37.0       3.6
          38.0       6.4
          39.0      13.8
          40.0       2.5
          41.0       5.3
          43.0       1.0
          44.0       7.5
          50.0       3.3
          51.0       8.5
          52.0      23.2
          53.0       6.1
          54.0       1.0
          61.0       2.4
          62.0       6.6
          63.0      18.1
          64.0      18.4
          65.0      15.4
          66.0       5.7
          67.0       2.6
          74.0       1.2
          75.0       3.7
          76.0       4.4
          77.0       4.8
          78.0       7.1
          79.0       8.1
          89.0       1.8
          90.0       6.2
          91.0      33.8
          92.0       7.4
          93.0       1.7
          96.0       1.3
         103.0       1.2
         105.0       3.2
         106.0       1.8
         107.0      10.0
         108.0       1.1
         119.0       2.0
         121.0      20.0
         122.0       2.0
         125.0       1.4
         137.0       2.2
         149.0       1.8
         153.0      14.4
         154.0       1.2
         165.0       1.0
         166.0       5.7
         167.0       2.2
         183.0     100.0
         184.0       8.1
         185.0       1.3
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C6 H5 N3 O4 0.039 g : 0.5 ml DMSO-d6
    2,6-dinitroaniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.489 B 8.42 C 6.839

         Hz     ppm     Int.
    

       3405.15   8.521     27
       3396.97   8.500    980
       3388.55   8.479   1000
       3363.40   8.416    299
       2741.33   6.860    324
       2733.03   6.839    606
       2728.03   6.827     25
       2724.73   6.818    307
    

in DMSO-d6



KBr disc



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