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MassMS2015-05133CW N-methyl-p-nitroaniline C7H8N2O2 (Mass of molecular ion: 152)
Source Temperature: 250 °C Sample Temperature: 20 °C Direct, 70 eV
15.0 2.9 18.0 1.7 26.0 1.2 27.0 3.2 28.0 9.7 30.0 7.8 37.0 2.3 38.0 5.6 39.0 10.7 40.0 1.6 41.0 3.0 42.0 2.8 46.0 2.7 50.0 15.0 51.0 12.3 52.0 8.2 53.0 4.9 54.0 3.3 55.0 2.6 61.0 1.8 62.0 4.4 63.0 13.0 64.0 10.4 65.0 30.3 66.0 4.9 67.0 2.9 68.0 1.5 73.0 1.0 74.0 6.4 75.0 5.0 76.0 10.2 77.0 43.2 78.0 15.4 79.0 29.3 80.0 4.1 90.0 3.9 91.0 7.3 92.0 1.6 93.0 1.5 94.0 16.0 95.0 1.1 104.0 10.1 105.0 17.8 106.0 27.8 107.0 2.5 120.0 1.5 122.0 57.6 123.0 4.7 136.0 5.3 150.0 1.9 151.0 3.7 152.0 100.0 153.0 10.2
400 MHz in DMSO-d6
90 MHz in CDCl3
in CDCl3
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1H NMR 399.65 MHz C7 H8 N2 O2 0.033 g : 0.5 ml DMSO-d6 N-methyl-p-nitroaniline 
Assign. Shift(ppm)
A 8.022 B 7.32 C 6.615 D 2.811 90MHZ:HSP-03-231 IN CDCL3
Hz ppm Int.3210.69 8.034 329 3208.74 8.029 119 3203.37 8.016 127 3201.42 8.011 339 2928.71 7.329 63 2923.95 7.317 62 2653.32 6.640 35 2648.56 6.628 347 2646.48 6.622 124 2644.04 6.616 54 2641.24 6.609 125 2639.16 6.604 337 1126.10 2.818 1000 1120.97 2.805 997
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1H NMR 89.56 MHz C7 H8 N2 O2 0.034 g : 0.5 ml CDCl3 N-methyl-p-nitroaniline Assign. Shift(ppm)
A 8.087 B 6.529 C 4.7 D 2.938
Hz ppm Int.732.31 8.177 22 729.13 8.142 233 727.00 8.118 64 721.94 8.061 68 719.81 8.038 257 716.63 8.002 27 589.25 6.580 224 587.06 6.555 61 582.06 6.500 51 579.94 6.476 195 263.13 2.939 1000
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in DMSO-d6
in CDCl3
KBr disc
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