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MassMS-IW-7274 L-lysine C6H14N2O2 (Mass of molecular ion: 146)
Source Temperature: 210 °C Sample Temperature: 190 °C Direct, 75 eV
15.0 2.6 16.0 6.3 17.0 17.5 18.0 70.6 26.0 7.8 27.0 24.4 28.0 52.0 29.0 11.7 30.0 95.4 31.0 2.7 37.0 1.2 38.0 2.4 39.0 13.0 40.0 6.2 41.0 29.4 42.0 20.0 43.0 42.8 44.0 38.2 45.0 4.4 46.0 1.4 50.0 3.8 51.0 5.9 52.0 14.3 53.0 8.9 54.0 18.3 55.0 33.6 56.0 100.0 57.0 20.4 58.0 6.1 59.0 6.0 65.0 3.4 66.0 5.7 67.0 11.4 68.0 7.1 69.0 6.5 70.0 19.4 71.0 15.3 72.0 66.6 73.0 6.6 74.0 13.1 75.0 3.7 77.0 2.1 78.0 3.7 79.0 13.8 80.0 8.1 81.0 7.8 82.0 35.7 83.0 83.6 84.0 74.6 85.0 6.7 86.0 1.5 87.0 1.9 88.0 1.9 89.0 1.8 92.0 2.0 93.0 6.9 94.0 1.6 95.0 1.7 96.0 1.1 97.0 1.8 98.0 3.0 99.0 16.4 100.0 9.3 101.0 3.8 104.0 3.2 107.0 1.7 108.0 2.8 109.0 2.4 110.0 11.4 111.0 18.9 112.0 3.4 117.0 2.5 126.0 1.5 127.0 2.8 128.0 8.8 129.0 10.8 130.0 4.7 147.0 1.7
90 MHz in D2O
400 MHz in D2O
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1H NMR 89.56 MHz C6 H14 N2 O2 0.041 g : 0.5 ml D2O L-lysine 
Assign. Shift(ppm)
B 3.756 C 3.029 D 1.95 to 1.43 THE SOLVENT SIGNAL REMOVED.
Hz ppm Int.342.94 3.830 384 337.25 3.766 907 331.19 3.698 554 279.25 3.119 559 272.56 3.044 1000 265.00 2.959 901 167.38 1.869 691 164.69 1.839 535 163.94 1.831 542 161.63 1.805 666 157.81 1.763 544 157.44 1.758 547 157.13 1.755 545 155.13 1.733 522 149.19 1.666 547 148.75 1.661 546 148.19 1.655 539 144.38 1.613 628 143.00 1.597 547 142.50 1.592 540 141.75 1.583 540
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1H NMR 399.65 MHz C6 H14 N2 O2 0.044 g : 0.5 ml D2O L-lysine Assign. Shift(ppm)
B 3.444 C 2.985 D 1.73 E 1.68 F 1.43 THE SOLVENT SIGNAL REMOVED.
Hz ppm Int.1382.93 3.461 355 1376.59 3.445 673 1370.48 3.430 374 1200.56 3.005 793 1196.29 2.994 229 1193.12 2.986 1000 1185.42 2.967 827 699.58 1.751 360 697.39 1.746 234 693.60 1.736 274 691.41 1.731 338 689.58 1.726 473 685.18 1.715 290 683.35 1.710 577 681.03 1.705 451 678.59 1.698 223 676.76 1.694 296 673.46 1.686 633 665.89 1.667 505 658.45 1.648 251 580.44 1.453 240 573.49 1.435 340 568.24 1.422 225 565.67 1.416 314 564.70 1.413 300 556.64 1.393 200
in D2O (PH 10.70)
in D2O (PH 1.68)
in D2O (PH 7.22)
KBr disc
nujol mull
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