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MassMS-NW-8661 5-acetyl-2-norbornene C9H12O (Mass of molecular ion: 136)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.8 27.0 4.7 38.0 1.3 39.0 9.5 40.0 3.8 41.0 3.3 43.0 20.4 50.0 1.1 51.0 2.7 52.0 1.0 53.0 1.7 55.0 6.6 58.0 7.7 63.0 1.6 65.0 7.8 66.0 100.0 67.0 6.3 71.0 16.9 77.0 10.1 78.0 5.5 79.0 2.7 91.0 9.6 92.0 2.1 93.0 14.6 94.0 1.5 121.0 1.1 136.0 10.8 137.0 1.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H12 O 0.05 ml : 0.5 ml CDCl3 5-acetyl-2-norbornene 
Assign. Shift(ppm)
A 6.145 B 5.852 C 3.241 D 3.015 E 2.894 F 2.126 G *1 1.745 J *1 1.49 K *2 1.45 L *2 1.330 ASSIGNED BY C-H COSY
Hz ppm Int.2460.57 6.157 82 2457.52 6.150 86 2454.96 6.143 96 2451.78 6.135 95 2343.26 5.864 91 2340.45 5.857 95 2337.52 5.849 88 2334.72 5.842 86 1295.41 3.242 97 1213.50 3.037 53 1209.59 3.027 89 1205.57 3.017 63 1204.59 3.015 71 1200.56 3.005 92 1196.78 2.995 57 1156.49 2.894 94 849.85 2.127 957 849.49 2.126 1000 710.08 1.777 59 706.30 1.768 59 701.05 1.755 53 698.49 1.748 79 697.39 1.746 66 694.70 1.739 72 689.58 1.726 61 685.79 1.716 63 604.00 1.512 59 601.44 1.505 74 599.98 1.502 65 597.29 1.495 71 592.65 1.483 43 592.16 1.482 43 589.97 1.477 71 589.48 1.475 69 588.62 1.473 46 588.01 1.472 50 585.33 1.465 132 583.37 1.460 62 580.93 1.454 31 579.10 1.450 56 577.15 1.445 98 574.71 1.439 83 572.75 1.434 42 535.52 1.340 124 534.91 1.339 102 534.18 1.337 80 529.05 1.324 57 527.47 1.320 97 526.00 1.317 61
in CDCl3
liquid film
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