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网站主页CAS数据库列表 5063-03-6更多图谱2-乙酰基-5-降冰片烯 (5063-03-6)红外图谱(IR1)

2-乙酰基-5-降冰片烯

产品名称 2-乙酰基-5-降冰片烯

CAS号5063-03-6

分子式C9H12O

分子量136.19

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  • Mass

    MS-NW-8661          
    5-acetyl-2-norbornene
    C9H12O              (Mass of molecular ion:    136)
    

       Source Temperature: 260 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       1.8
          27.0       4.7
          38.0       1.3
          39.0       9.5
          40.0       3.8
          41.0       3.3
          43.0      20.4
          50.0       1.1
          51.0       2.7
          52.0       1.0
          53.0       1.7
          55.0       6.6
          58.0       7.7
          63.0       1.6
          65.0       7.8
          66.0     100.0
          67.0       6.3
          71.0      16.9
          77.0      10.1
          78.0       5.5
          79.0       2.7
          91.0       9.6
          92.0       2.1
          93.0      14.6
          94.0       1.5
         121.0       1.1
         136.0      10.8
         137.0       1.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C9 H12 O 0.05 ml : 0.5 ml CDCl3
    5-acetyl-2-norbornene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.145 B 5.852 C 3.241 D 3.015 E 2.894 F 2.126 G *1 1.745 J *1 1.49 K *2 1.45 L *2 1.330 ASSIGNED BY C-H COSY

         Hz     ppm     Int.
    

       2460.57   6.157     82
       2457.52   6.150     86
       2454.96   6.143     96
       2451.78   6.135     95
       2343.26   5.864     91
       2340.45   5.857     95
       2337.52   5.849     88
       2334.72   5.842     86
       1295.41   3.242     97
       1213.50   3.037     53
       1209.59   3.027     89
       1205.57   3.017     63
       1204.59   3.015     71
       1200.56   3.005     92
       1196.78   2.995     57
       1156.49   2.894     94
        849.85   2.127    957
        849.49   2.126   1000
        710.08   1.777     59
        706.30   1.768     59
        701.05   1.755     53
        698.49   1.748     79
        697.39   1.746     66
        694.70   1.739     72
        689.58   1.726     61
        685.79   1.716     63
        604.00   1.512     59
        601.44   1.505     74
        599.98   1.502     65
        597.29   1.495     71
        592.65   1.483     43
        592.16   1.482     43
        589.97   1.477     71
        589.48   1.475     69
        588.62   1.473     46
        588.01   1.472     50
        585.33   1.465    132
        583.37   1.460     62
        580.93   1.454     31
        579.10   1.450     56
        577.15   1.445     98
        574.71   1.439     83
        572.75   1.434     42
        535.52   1.340    124
        534.91   1.339    102
        534.18   1.337     80
        529.05   1.324     57
        527.47   1.320     97
        526.00   1.317     61
    

in CDCl3



liquid film