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MassMS-IW-9730 6-bromo-2,4-xylidine C8H10BrN (Mass of molecular ion: 199)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 3.1 28.0 5.0 30.0 1.5 38.0 1.9 39.0 8.2 40.0 1.3 41.0 3.6 42.0 3.9 45.5 2.1 46.5 4.8 50.0 3.3 51.0 7.9 52.0 8.4 53.0 4.7 54.0 2.6 58.5 11.9 59.0 3.1 59.5 7.8 60.0 4.8 62.0 1.9 63.0 4.2 64.0 1.5 65.0 9.2 66.0 2.3 67.0 1.0 74.0 1.0 75.0 1.7 76.0 2.6 77.0 12.3 78.0 5.0 79.0 2.3 80.0 2.4 89.0 2.6 90.0 2.1 91.0 16.2 92.0 6.6 93.0 6.7 94.0 1.3 99.5 3.6 100.5 3.2 102.0 1.9 103.0 5.1 104.0 6.5 105.0 3.4 106.0 3.5 116.0 1.5 117.0 3.8 118.0 13.9 119.0 10.4 120.0 74.4 121.0 12.0 184.0 18.4 185.0 1.7 186.0 17.7 187.0 1.5 198.0 39.6 199.0 100.0 200.0 47.4 201.0 96.6 202.0 8.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H10 Br N 0.041 g : 0.5 ml CDCl3 6-bromo-2,4-xylidine 
Assign. Shift(ppm)
A 7.114 B 6.802 C 3.88 D *1 2.189 E *1 2.164
Hz ppm Int.2844.85 7.119 129 2844.24 7.117 173 2843.63 7.116 179 2842.90 7.114 186 2842.29 7.112 184 2841.67 7.111 146 2720.09 6.807 129 2719.36 6.805 177 2718.75 6.803 179 2718.02 6.802 181 2717.41 6.800 181 2716.67 6.798 139 1552.00 3.884 41 875.12 2.190 1000 864.87 2.165 971
in CDCl3
KBr disk
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