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MassMS-IW-9731 4-bromo-2,6-xylidine C8H10BrN (Mass of molecular ion: 199)
Source Temperature: 230 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 2.8 28.0 5.4 30.0 3.2 38.0 1.9 39.0 7.3 41.0 2.6 42.0 6.3 45.5 1.3 46.5 5.3 50.0 3.0 51.0 6.9 52.0 5.2 53.0 3.8 54.0 3.8 58.5 12.8 59.0 2.5 59.5 6.6 60.0 5.9 62.0 2.2 63.0 5.0 64.0 1.6 65.0 7.5 66.0 2.0 74.0 1.1 75.0 1.6 76.0 1.9 77.0 14.8 78.0 4.3 79.0 2.7 80.0 2.2 89.0 2.4 90.0 2.0 91.0 15.6 92.0 7.4 93.0 7.8 94.0 1.5 99.5 5.5 100.5 4.9 102.0 3.0 103.0 10.5 104.0 5.7 105.0 2.6 106.0 1.5 117.0 2.7 118.0 8.3 119.0 10.4 120.0 85.9 121.0 10.0 184.0 5.7 186.0 5.2 198.0 20.5 199.0 100.0 200.0 28.8 201.0 97.4 202.0 8.8
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C8 H10 Br N 0.041 g : 0.5 ml CDCl3 4-bromo-2,6-xylidine 
Assign. Shift(ppm)
A 7.044 B 3.53 C 2.123
Hz ppm Int.2815.92 7.046 230 2815.19 7.045 276 2814.58 7.043 225 1413.33 3.537 46 849.37 2.126 751 848.75 2.124 1000 848.14 2.123 676
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1H NMR 89.56 MHz C8 H10 Br N 0.051 g : 0.5 ml CDCl3 4-bromo-2,6-xylidine Assign. Shift(ppm)
A 7.035 B 3.5 C 2.116
Hz ppm Int.630.13 7.036 256 314.31 3.510 33 189.63 2.118 1000
in CDCl3
KBr disc
nujol mull
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