2-溴-4,6-二甲基苯胺

Mass

MS-IW-9730          
6-bromo-2,4-xylidine
C8H10BrN            (Mass of molecular ion:    199)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       3.1
      28.0       5.0
      30.0       1.5
      38.0       1.9
      39.0       8.2
      40.0       1.3
      41.0       3.6
      42.0       3.9
      45.5       2.1
      46.5       4.8
      50.0       3.3
      51.0       7.9
      52.0       8.4
      53.0       4.7
      54.0       2.6
      58.5      11.9
      59.0       3.1
      59.5       7.8
      60.0       4.8
      62.0       1.9
      63.0       4.2
      64.0       1.5
      65.0       9.2
      66.0       2.3
      67.0       1.0
      74.0       1.0
      75.0       1.7
      76.0       2.6
      77.0      12.3
      78.0       5.0
      79.0       2.3
      80.0       2.4
      89.0       2.6
      90.0       2.1
      91.0      16.2
      92.0       6.6
      93.0       6.7
      94.0       1.3
      99.5       3.6
     100.5       3.2
     102.0       1.9
     103.0       5.1
     104.0       6.5
     105.0       3.4
     106.0       3.5
     116.0       1.5
     117.0       3.8
     118.0      13.9
     119.0      10.4
     120.0      74.4
     121.0      12.0
     184.0      18.4
     185.0       1.7
     186.0      17.7
     187.0       1.5
     198.0      39.6
     199.0     100.0
     200.0      47.4
     201.0      96.6
     202.0       8.7

Assign. Shift(ppm) A 7.114 B 6.802 C 3.88 D *1 2.189 E *1 2.164

     Hz     ppm     Int.

   2844.85   7.119    129
   2844.24   7.117    173
   2843.63   7.116    179
   2842.90   7.114    186
   2842.29   7.112    184
   2841.67   7.111    146
   2720.09   6.807    129
   2719.36   6.805    177
   2718.75   6.803    179
   2718.02   6.802    181
   2717.41   6.800    181
   2716.67   6.798    139
   1552.00   3.884     41
    875.12   2.190   1000
    864.87   2.165    971