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MS-NW-7706 p-(p-tolyloxy)aniline C13H13NO (Mass of molecular ion: 199)
Source Temperature: 270 °C Sample Temperature: 170 °C Reservoir, 75 eV
27.0 1.5 28.0 1.5 39.0 6.3 41.0 1.8 50.0 1.2 51.0 2.6 52.0 2.6 53.0 4.0 54.0 1.2 63.0 3.1 64.0 1.5 65.0 12.3 66.0 1.4 77.0 1.9 79.0 1.1 80.0 10.0 81.0 1.0 89.0 2.0 90.0 1.0 91.0 7.7 92.0 3.9 93.0 1.2 107.0 1.3 108.0 57.1 109.0 6.1 119.0 1.0 128.0 1.4 143.0 1.3 156.0 5.4 170.0 7.2 171.0 2.0 198.0 3.2 199.0 100.0 200.0 14.8 201.0 1.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C13 H13 N O 0.039 g : 0.5 ml CDCl3 p-(p-tolyloxy)aniline Assign. Shift(ppm)
A 7.071 B 6.84 C 6.83 D 6.644 E 3.5 F 2.291
Hz ppm Int.
2833.62 7.091 34 2832.89 7.089 38 2830.81 7.084 208 2830.08 7.082 235 2822.02 7.062 278 2821.53 7.061 262 2741.94 6.861 58 2738.53 6.853 411 2736.33 6.847 181 2734.74 6.843 411 2732.18 6.837 231 2729.86 6.831 515 2728.39 6.827 171 2726.20 6.822 379 2723.39 6.815 54 2662.84 6.663 62 2659.42 6.655 506 2657.23 6.649 155 2652.83 6.638 142 2650.76 6.633 386 2647.22 6.624 45 915.89 2.292 1000
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