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MS-IW-6967 4,4'-(4,4'-biphenylylenedioxy)dianiline C24H20N2O2 (Mass of molecular ion: 368)
Source Temperature: 200 °C Sample Temperature: 250 °C Direct, 75 eV
39.0 1.1 53.0 1.0 65.0 4.3 80.0 5.7 92.0 1.4 108.0 28.8 109.0 2.6 139.0 1.8 152.0 2.8 184.0 10.1 184.5 2.7 230.0 1.1 231.0 1.0 232.0 1.0 248.0 1.0 260.0 2.1 261.0 1.2 276.0 2.8 339.0 2.3 340.0 1.3 367.0 2.1 368.0 100.0 369.0 26.9 370.0 4.0
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C24 H20 N2 O2 0.041 g : 0.5 ml DMSO-d6 4,4'-(4,4'-biphenylylenedioxy)dianiline Assign. Shift(ppm)
A 7.525 B 6.914 C 6.809 D 6.633 E 5.01
Hz ppm Int.
3015.14 7.545 86 3012.21 7.538 728 3010.01 7.532 241 3005.49 7.521 256 3003.30 7.515 787 3000.24 7.508 87 2770.51 6.933 92 2767.58 6.926 817 2765.38 6.920 248 2760.86 6.909 249 2758.67 6.903 779 2755.74 6.896 77 2729.61 6.831 71 2726.32 6.822 797 2724.12 6.817 250 2719.73 6.806 283 2717.53 6.800 989 2714.11 6.792 97 2657.96 6.651 103 2654.66 6.643 1000 2652.47 6.637 266 2648.07 6.626 254 2645.87 6.621 752 2642.46 6.612 69 2000.85 5.007 769
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