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网站主页CAS数据库列表 3840-18-4更多图谱2-甲基-2'-氨基二苯醚(3840-18-4)红外图谱(IR1)

2-甲基-2'-氨基二苯醚

产品名称 2-甲基-2'-氨基二苯醚

CAS号3840-18-4

分子式C13H13NO

分子量199.25

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  • Mass

    MS-NW-6664          
    o-(o-tolyloxy)aniline
    C13H13NO            (Mass of molecular ion:    199)
    

       Source Temperature: 250 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          27.0       2.1
          28.0       1.4
          38.0       1.1
          39.0       7.4
          41.0       1.8
          50.0       1.3
          51.0       3.6
          52.0       4.1
          53.0       4.6
          54.0       1.1
          63.0       3.3
          64.0       2.0
          65.0      11.9
          66.0       1.9
          77.0       2.8
          78.0       1.6
          79.0       3.1
          80.0      17.3
          81.0       1.4
          89.0       2.0
          90.0       1.1
          91.0      10.2
          92.0       5.2
          93.0      42.1
          94.0       3.6
         104.0       1.1
         106.0       5.3
         107.0       1.8
         108.0      20.1
         109.0       2.7
         128.0       1.6
         129.0       1.1
         130.0       1.3
         153.0       1.1
         154.0       1.7
         155.0       1.0
         156.0       1.8
         167.0       1.4
         170.0       2.5
         180.0       3.6
         181.0       6.4
         182.0       4.9
         183.0       4.5
         184.0       5.0
         185.0       1.1
         196.0       1.3
         198.0       6.0
         199.0     100.0
         200.0      14.4
         201.0       1.3
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C13 H13 N O 0.05 ml : 0.5 ml CDCl3
    o-(o-tolyloxy)aniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.203 B 7.081 C 6.983 D 6.893 E 6.780 F 6.752 G 6.66 J 6.634 K 3.73 L 2.281

         Hz     ppm     Int.
    

       2881.84   7.211    119
       2875.49   7.196    129
       2874.51   7.193    139
       2838.62   7.103     54
       2836.91   7.099     58
       2831.05   7.084    120
       2829.47   7.080    126
       2823.24   7.065     88
       2821.78   7.061     85
       2797.61   7.001    109
       2796.26   6.997    126
       2790.16   6.982    160
       2788.94   6.979    181
       2782.71   6.963     69
       2781.49   6.960     75
       2763.31   6.915     84
       2761.23   6.910     91
       2760.99   6.909     91
       2756.47   6.898     99
       2755.25   6.895    129
       2754.52   6.893    132
       2753.42   6.890    138
       2748.66   6.878    119
       2746.70   6.873    133
       2714.23   6.792    168
       2713.13   6.789    182
       2706.18   6.772    156
       2705.08   6.769    169
       2702.64   6.763    195
       2701.29   6.760    218
       2694.95   6.744    160
       2693.36   6.740    174
       2667.72   6.676     54
       2665.77   6.671     99
       2659.79   6.656    273
       2657.59   6.650    407
       2656.13   6.647    244
       2650.76   6.633    158
       2649.29   6.630    186
       2648.19   6.627     76
       2642.70   6.613     53
       2641.36   6.610     56
       1488.77   3.726    157
        911.62   2.282   1000
    

in CDCl3



liquid film