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MassMS-NW-7047 N,N'-disalicylidene-1,6-hexanediamine C20H24N2O2 (Mass of molecular ion: 324)
Source Temperature: 180 °C Sample Temperature: 130 °C Direct, 75 eV
18.0 1.1 27.0 3.4 28.0 7.6 29.0 3.8 30.0 3.2 39.0 8.6 40.0 1.2 41.0 17.8 42.0 3.1 43.0 2.7 44.0 1.6 50.0 1.5 51.0 8.5 52.0 2.8 53.0 3.3 54.0 2.7 55.0 9.7 56.0 4.7 57.0 1.1 63.0 2.0 64.0 1.7 65.0 9.0 66.0 4.2 67.0 3.1 68.0 1.7 69.0 3.3 70.0 3.4 76.0 1.7 77.0 22.5 78.0 9.5 79.0 7.8 80.0 1.9 81.0 2.0 82.0 4.1 83.0 3.3 84.0 7.6 89.0 1.0 90.0 1.2 91.0 5.4 92.0 2.7 93.0 7.9 94.0 2.4 95.0 4.4 96.0 8.5 97.0 3.5 98.0 2.0 102.0 4.0 103.0 2.7 104.0 3.0 105.0 5.5 106.0 4.3 107.0 49.1 108.0 5.2 116.0 1.6 117.0 2.3 118.0 6.0 119.0 3.9 120.0 21.1 121.0 22.6 122.0 21.8 123.0 3.1 130.0 1.1 131.0 6.0 132.0 6.9 133.0 6.6 134.0 24.4 135.0 19.1 136.0 6.7 145.0 1.0 146.0 4.6 147.0 3.9 148.0 60.3 149.0 17.9 150.0 2.3 158.0 1.1 160.0 6.7 161.0 2.5 162.0 27.9 163.0 6.3 172.0 1.0 174.0 6.3 175.0 5.3 176.0 15.7 177.0 4.7 186.0 14.1 187.0 2.4 188.0 8.4 189.0 3.8 190.0 11.9 191.0 1.7 200.0 2.3 201.0 2.1 202.0 74.4 203.0 100.0 204.0 24.1 205.0 28.0 206.0 4.5 217.0 3.6 227.0 1.0 324.0 36.7 325.0 8.7 326.0 1.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C20 H24 N2 O2 0.038 g : 0.5 ml CDCl3 N,N'-disalicylidene-1,6-hexanediamine 
Assign. Shift(ppm)
A 13.6 B 8.313 C 7.285 D 7.224 E 6.949 F 6.855 G 3.572 J 1.699 K 1.426
Hz ppm Int.5456.89 13.655 89 3322.46 8.314 992 2920.96 7.309 258 2919.12 7.305 294 2913.63 7.291 332 2912.53 7.288 429 2911.98 7.287 455 2910.88 7.284 407 2905.39 7.270 319 2903.56 7.266 370 2892.02 7.237 484 2890.37 7.233 457 2884.32 7.218 553 2882.67 7.213 495 2781.20 6.960 607 2773.87 6.941 518 2773.32 6.940 540 2772.96 6.939 540 2747.31 6.875 386 2746.22 6.872 386 2739.80 6.856 597 2738.89 6.854 611 2735.23 6.845 38 2732.29 6.837 327 2731.38 6.835 323 1435.11 3.591 457 1434.01 3.589 487 1428.33 3.574 963 1427.23 3.572 1000 1421.56 3.558 498 1420.46 3.555 508 685.96 1.717 283 679.18 1.700 440 674.60 1.688 253 672.04 1.682 322 666.36 1.668 106 665.26 1.665 107 577.34 1.445 316 573.86 1.436 390 570.01 1.427 687 566.35 1.418 377 562.69 1.408 261
in CDCl3
KBr disc
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