图谱信息 供应商 相关产品
网站主页CAS数据库列表 4081-35-0更多图谱N,N'-双(亚水杨基)-1,6-己烷二胺(4081-35-0)核磁图(13CNMR)

N,N'-双(亚水杨基)-1,6-己烷二胺

产品名称 N,N'-双(亚水杨基)-1,6-己烷二胺

CAS号4081-35-0

分子式C20H24N2O2

分子量324.42

展开


  • Mass

    MS-NW-7047          
    N,N'-disalicylidene-1,6-hexanediamine
    C20H24N2O2          (Mass of molecular ion:    324)
    

       Source Temperature: 180 °C
       Sample Temperature: 130 °C
       Direct, 75 eV
    

          18.0       1.1
          27.0       3.4
          28.0       7.6
          29.0       3.8
          30.0       3.2
          39.0       8.6
          40.0       1.2
          41.0      17.8
          42.0       3.1
          43.0       2.7
          44.0       1.6
          50.0       1.5
          51.0       8.5
          52.0       2.8
          53.0       3.3
          54.0       2.7
          55.0       9.7
          56.0       4.7
          57.0       1.1
          63.0       2.0
          64.0       1.7
          65.0       9.0
          66.0       4.2
          67.0       3.1
          68.0       1.7
          69.0       3.3
          70.0       3.4
          76.0       1.7
          77.0      22.5
          78.0       9.5
          79.0       7.8
          80.0       1.9
          81.0       2.0
          82.0       4.1
          83.0       3.3
          84.0       7.6
          89.0       1.0
          90.0       1.2
          91.0       5.4
          92.0       2.7
          93.0       7.9
          94.0       2.4
          95.0       4.4
          96.0       8.5
          97.0       3.5
          98.0       2.0
         102.0       4.0
         103.0       2.7
         104.0       3.0
         105.0       5.5
         106.0       4.3
         107.0      49.1
         108.0       5.2
         116.0       1.6
         117.0       2.3
         118.0       6.0
         119.0       3.9
         120.0      21.1
         121.0      22.6
         122.0      21.8
         123.0       3.1
         130.0       1.1
         131.0       6.0
         132.0       6.9
         133.0       6.6
         134.0      24.4
         135.0      19.1
         136.0       6.7
         145.0       1.0
         146.0       4.6
         147.0       3.9
         148.0      60.3
         149.0      17.9
         150.0       2.3
         158.0       1.1
         160.0       6.7
         161.0       2.5
         162.0      27.9
         163.0       6.3
         172.0       1.0
         174.0       6.3
         175.0       5.3
         176.0      15.7
         177.0       4.7
         186.0      14.1
         187.0       2.4
         188.0       8.4
         189.0       3.8
         190.0      11.9
         191.0       1.7
         200.0       2.3
         201.0       2.1
         202.0      74.4
         203.0     100.0
         204.0      24.1
         205.0      28.0
         206.0       4.5
         217.0       3.6
         227.0       1.0
         324.0      36.7
         325.0       8.7
         326.0       1.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C20 H24 N2 O2 0.038 g : 0.5 ml CDCl3
    N,N'-disalicylidene-1,6-hexanediamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 13.6 B 8.313 C 7.285 D 7.224 E 6.949 F 6.855 G 3.572 J 1.699 K 1.426

         Hz     ppm     Int.
    

       5456.89  13.655     89
       3322.46   8.314    992
       2920.96   7.309    258
       2919.12   7.305    294
       2913.63   7.291    332
       2912.53   7.288    429
       2911.98   7.287    455
       2910.88   7.284    407
       2905.39   7.270    319
       2903.56   7.266    370
       2892.02   7.237    484
       2890.37   7.233    457
       2884.32   7.218    553
       2882.67   7.213    495
       2781.20   6.960    607
       2773.87   6.941    518
       2773.32   6.940    540
       2772.96   6.939    540
       2747.31   6.875    386
       2746.22   6.872    386
       2739.80   6.856    597
       2738.89   6.854    611
       2735.23   6.845     38
       2732.29   6.837    327
       2731.38   6.835    323
       1435.11   3.591    457
       1434.01   3.589    487
       1428.33   3.574    963
       1427.23   3.572   1000
       1421.56   3.558    498
       1420.46   3.555    508
        685.96   1.717    283
        679.18   1.700    440
        674.60   1.688    253
        672.04   1.682    322
        666.36   1.668    106
        665.26   1.665    107
        577.34   1.445    316
        573.86   1.436    390
        570.01   1.427    687
        566.35   1.418    377
        562.69   1.408    261
    

in CDCl3



KBr disc



nujol mull