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MS-IW-3683 p-fluoro-N,N-dimethylaniline C8H10FN (Mass of molecular ion: 139)
Source Temperature: 220 °C Sample Temperature: 160 °C Reservoir, 75 eV
15.0 1.1 39.0 1.1 42.0 5.3 44.0 1.2 50.0 2.1 51.0 1.9 57.0 2.8 61.0 2.1 63.0 1.3 69.0 3.8 69.5 3.8 70.0 1.3 74.0 1.3 75.0 6.8 77.0 1.9 81.0 1.1 83.0 2.5 91.0 1.9 94.0 1.0 95.0 15.1 96.0 5.8 97.0 3.8 108.0 1.5 109.0 4.3 110.0 2.5 111.0 1.3 117.0 1.1 121.0 1.0 122.0 15.4 123.0 17.4 124.0 4.5 136.0 4.9 137.0 1.8 138.0 100.0 139.0 71.6 140.0 6.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H10 F N 0.039 g : 0.5 ml CDCl3 p-fluoro-N,N-dimethylaniline Assign. Shift(ppm)
A 6.933 B 6.668 C 2.882
Hz ppm Int.
2780.64 6.958 75 2778.20 6.952 28 2773.80 6.941 32 2771.36 6.935 124 2769.90 6.931 37 2765.38 6.920 31 2762.94 6.914 102 2671.63 6.685 87 2669.31 6.680 29 2667.24 6.674 89 2664.79 6.668 48 2662.48 6.663 77 2660.40 6.657 29 2658.08 6.652 78 1151.73 2.882 1000
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