1-(4-氟苯基)哌嗪

Mass

MS-IW-0587          
1-(p-fluorophenyl)piperazine
C10H13FN2           (Mass of molecular ion:    180)

   Source Temperature: 260 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      18.0       1.5
      27.0       1.2
      28.0       7.0
      29.0       4.9
      30.0       3.0
      41.0       1.1
      42.0       3.2
      43.0       1.0
      56.0       9.8
      57.0       5.3
      70.0       1.3
      75.0       4.0
      83.0       1.4
      95.0       9.5
      96.0       1.8
      97.0       1.1
     109.0       4.9
     110.0       1.0
     111.0       1.0
     122.0      12.4
     123.0      12.2
     124.0       4.7
     125.0       1.1
     136.0       1.2
     138.0     100.0
     139.0       9.2
     150.0       1.9
     180.0      25.2
     181.0       3.3
     193.0       1.9

Assign. Shift(ppm) A 6.947 B 6.854 C 3.034 D 3.003 E 2.21 ASSIGNED BY C-H COSY.

     Hz     ppm     Int.

   2789.67   6.981     38
   2786.01   6.972    383
   2783.45   6.965    144
   2781.37   6.960     59
   2779.17   6.955    204
   2777.71   6.951    481
   2776.86   6.949    612
   2775.27   6.945    185
   2772.95   6.939     94
   2770.87   6.934    182
   2768.55   6.928    559
   2764.77   6.918     82
   2748.78   6.878     70
   2745.12   6.869    518
   2742.68   6.863    180
   2740.48   6.858    529
   2738.16   6.852    257
   2735.96   6.846    340
   2733.64   6.841    143
   2731.32   6.835    317
   2727.66   6.826     40
   1219.48   3.052    245
   1217.53   3.047    325
   1215.45   3.042    454
   1213.13   3.036    486
   1211.06   3.031    650
   1209.11   3.026    977
   1203.74   3.012   1000
   1201.54   3.007    604
   1199.34   3.001    485
   1197.14   2.996    460
   1194.82   2.990    324
   1192.99   2.986    256
    881.71   2.207    184