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网站主页CAS数据库列表 371-40-4更多图谱4-氟苯胺(371-40-4)核磁图(13CNMR)

4-氟苯胺

产品名称 4-氟苯胺

CAS号371-40-4

分子式C6H6FN

分子量111.12

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  • Mass

    MS-NW-0998          
    p-fluoroaniline
    C6H6FN              (Mass of molecular ion:    111)
    

       Source Temperature: 250 °C
       Sample Temperature: 130 °C
       Reservoir, 75 eV
    

          28.0       3.9
          31.0       1.8
          37.0       1.1
          38.0       1.5
          39.0       2.4
          41.0       2.6
          45.5       1.1
          50.0       1.3
          51.0       1.3
          52.0       2.7
          55.5       3.6
          56.0       1.5
          57.0       6.7
          58.0       1.1
          61.0       1.1
          62.0       1.4
          63.0       3.4
          64.0       6.4
          65.0       2.5
          75.0       1.0
          81.0       1.7
          82.0       1.7
          83.0      18.3
          84.0      30.1
          85.0       2.9
          91.0       3.9
          94.0       1.1
         110.0       6.1
         111.0     100.0
         112.0       6.9
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H6 F N 0.02 ml : 0.5 ml CDCl3
    p-fluoroaniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.82 B 6.59 C 3.45 J(A,B)=9.2HZ J(A,F-19)=9.0HZ J(B,F-19)=4.7HZ

         Hz     ppm     Int.
    

        621.94   6.945    461
        621.44   6.939    254
        619.44   6.917    177
        615.38   6.872    228
        613.00   6.845   1000
        611.00   6.823    207
        609.69   6.808    144
        607.00   6.778    216
        604.44   6.749    842
        601.38   6.715    151
        599.38   6.693    128
        596.25   6.658    842
        594.63   6.640    195
        593.69   6.629    243
        591.63   6.606    843
        589.56   6.583    258
        589.00   6.577    251
        587.56   6.561    325
        587.06   6.555    451
        585.00   6.532    168
        583.81   6.519     76
        582.94   6.509    278
        582.38   6.503    370
        308.63   3.447    655
    

in CDCl3



liquid film