1-氨基-2,6-二甲基哌啶

Mass

MS-NW-5767          
1-amino-2,6-dimethylpiperidine
C7H16N2             (Mass of molecular ion:    128)

   Source Temperature: 250 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       2.3
      18.0       5.8
      27.0       7.1
      28.0       3.3
      29.0       5.2
      30.0       4.5
      31.0       2.1
      39.0       6.6
      40.0       1.6
      41.0      16.6
      42.0      13.0
      43.0       7.4
      44.0       4.5
      45.0       1.9
      53.0       1.8
      54.0       2.2
      55.0      11.4
      56.0       4.5
      57.0      19.4
      58.0      24.5
      59.0       6.4
      67.0       1.4
      68.0       4.1
      69.0       6.2
      70.0       5.8
      71.0       3.3
      72.0       1.2
      81.0       1.9
      82.0       1.3
      83.0       4.2
      84.0       1.3
      85.0       1.6
      96.0       2.2
      98.0       2.8
      99.0       1.1
     107.0       1.5
     111.0       2.5
     112.0       1.5
     113.0     100.0
     114.0       8.1
     127.0       2.7
     128.0      21.1
     129.0       1.9

Assign. Shift(ppm) A 2.91 B 2.08 C 1.79 to 1.00 D 1.214

     Hz     ppm     Int.

    260.56   2.910     93
    191.63   2.140     41
    191.13   2.135     46
    190.56   2.128     46
    189.06   2.111     33
    187.13   2.090     34
    186.63   2.084     32
    185.81   2.075     30
    184.44   2.060     33
    183.69   2.052     30
    179.13   2.001     31
    175.13   1.956     59
    154.88   1.730     36
    152.81   1.707     44
    151.75   1.695     48
    151.00   1.687     60
    149.75   1.673     35
    148.94   1.664     45
    148.38   1.657     42
    147.50   1.647     48
    147.00   1.642     47
    146.25   1.633     60
    144.50   1.614     71
    143.00   1.597     79
    140.94   1.574     67
    140.06   1.564     61
    138.50   1.547     38
    137.25   1.533     55
    136.31   1.522     43
    134.00   1.497     45
    133.56   1.492     45
    132.81   1.483     46
    131.44   1.468     43
    130.94   1.463     38
    130.63   1.459     38
    129.44   1.446     49
    128.06   1.430     55
    127.56   1.425     55
    126.00   1.407     58
    124.38   1.389     67
    123.81   1.383     65
    122.88   1.373     49
    122.25   1.366     42
    121.38   1.356     40
    119.50   1.335     64
    118.44   1.323     68
    117.56   1.313     86
    115.31   1.288     37
    113.88   1.272     42
    111.38   1.244   1000
    108.00   1.206     31
    105.38   1.177    771