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MassMS-NW-5767 1-amino-2,6-dimethylpiperidine C7H16N2 (Mass of molecular ion: 128)
Source Temperature: 250 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 2.3 18.0 5.8 27.0 7.1 28.0 3.3 29.0 5.2 30.0 4.5 31.0 2.1 39.0 6.6 40.0 1.6 41.0 16.6 42.0 13.0 43.0 7.4 44.0 4.5 45.0 1.9 53.0 1.8 54.0 2.2 55.0 11.4 56.0 4.5 57.0 19.4 58.0 24.5 59.0 6.4 67.0 1.4 68.0 4.1 69.0 6.2 70.0 5.8 71.0 3.3 72.0 1.2 81.0 1.9 82.0 1.3 83.0 4.2 84.0 1.3 85.0 1.6 96.0 2.2 98.0 2.8 99.0 1.1 107.0 1.5 111.0 2.5 112.0 1.5 113.0 100.0 114.0 8.1 127.0 2.7 128.0 21.1 129.0 1.9
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H16 N2 0.04 ml : 0.5 ml CDCl3 1-amino-2,6-dimethylpiperidine 
Assign. Shift(ppm)
A 2.91 B 2.08 C 1.79 to 1.00 D 1.214
Hz ppm Int.260.56 2.910 93 191.63 2.140 41 191.13 2.135 46 190.56 2.128 46 189.06 2.111 33 187.13 2.090 34 186.63 2.084 32 185.81 2.075 30 184.44 2.060 33 183.69 2.052 30 179.13 2.001 31 175.13 1.956 59 154.88 1.730 36 152.81 1.707 44 151.75 1.695 48 151.00 1.687 60 149.75 1.673 35 148.94 1.664 45 148.38 1.657 42 147.50 1.647 48 147.00 1.642 47 146.25 1.633 60 144.50 1.614 71 143.00 1.597 79 140.94 1.574 67 140.06 1.564 61 138.50 1.547 38 137.25 1.533 55 136.31 1.522 43 134.00 1.497 45 133.56 1.492 45 132.81 1.483 46 131.44 1.468 43 130.94 1.463 38 130.63 1.459 38 129.44 1.446 49 128.06 1.430 55 127.56 1.425 55 126.00 1.407 58 124.38 1.389 67 123.81 1.383 65 122.88 1.373 49 122.25 1.366 42 121.38 1.356 40 119.50 1.335 64 118.44 1.323 68 117.56 1.313 86 115.31 1.288 37 113.88 1.272 42 111.38 1.244 1000 108.00 1.206 31 105.38 1.177 771
in CDCl3
liquid film
4880 A,200 M,liquid
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