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1-氨基-2,6-二甲基哌啶

产品名称 1-氨基-2,6-二甲基哌啶

CAS号39135-39-2

分子式C7H16N2

分子量128.22

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  • Mass

    MS-NW-5767          
    1-amino-2,6-dimethylpiperidine
    C7H16N2             (Mass of molecular ion:    128)
    

       Source Temperature: 250 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          15.0       2.3
          18.0       5.8
          27.0       7.1
          28.0       3.3
          29.0       5.2
          30.0       4.5
          31.0       2.1
          39.0       6.6
          40.0       1.6
          41.0      16.6
          42.0      13.0
          43.0       7.4
          44.0       4.5
          45.0       1.9
          53.0       1.8
          54.0       2.2
          55.0      11.4
          56.0       4.5
          57.0      19.4
          58.0      24.5
          59.0       6.4
          67.0       1.4
          68.0       4.1
          69.0       6.2
          70.0       5.8
          71.0       3.3
          72.0       1.2
          81.0       1.9
          82.0       1.3
          83.0       4.2
          84.0       1.3
          85.0       1.6
          96.0       2.2
          98.0       2.8
          99.0       1.1
         107.0       1.5
         111.0       2.5
         112.0       1.5
         113.0     100.0
         114.0       8.1
         127.0       2.7
         128.0      21.1
         129.0       1.9
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C7 H16 N2 0.04 ml : 0.5 ml CDCl3
    1-amino-2,6-dimethylpiperidine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.91 B 2.08 C 1.79 to 1.00 D 1.214

         Hz     ppm     Int.
    

        260.56   2.910     93
        191.63   2.140     41
        191.13   2.135     46
        190.56   2.128     46
        189.06   2.111     33
        187.13   2.090     34
        186.63   2.084     32
        185.81   2.075     30
        184.44   2.060     33
        183.69   2.052     30
        179.13   2.001     31
        175.13   1.956     59
        154.88   1.730     36
        152.81   1.707     44
        151.75   1.695     48
        151.00   1.687     60
        149.75   1.673     35
        148.94   1.664     45
        148.38   1.657     42
        147.50   1.647     48
        147.00   1.642     47
        146.25   1.633     60
        144.50   1.614     71
        143.00   1.597     79
        140.94   1.574     67
        140.06   1.564     61
        138.50   1.547     38
        137.25   1.533     55
        136.31   1.522     43
        134.00   1.497     45
        133.56   1.492     45
        132.81   1.483     46
        131.44   1.468     43
        130.94   1.463     38
        130.63   1.459     38
        129.44   1.446     49
        128.06   1.430     55
        127.56   1.425     55
        126.00   1.407     58
        124.38   1.389     67
        123.81   1.383     65
        122.88   1.373     49
        122.25   1.366     42
        121.38   1.356     40
        119.50   1.335     64
        118.44   1.323     68
        117.56   1.313     86
        115.31   1.288     37
        113.88   1.272     42
        111.38   1.244   1000
        108.00   1.206     31
        105.38   1.177    771
    

in CDCl3



liquid film



4880 A,200 M,liquid