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网站主页CAS数据库列表 372-19-0更多图谱3-氟苯胺(372-19-0)红外图谱(IR1)

3-氟苯胺

产品名称 3-氟苯胺

CAS号372-19-0

分子式C6H6FN

分子量111.12

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  • Mass

    MS-NW-1008          
    m-fluoroaniline
    C6H6FN              (Mass of molecular ion:    111)
    

       Source Temperature: 260 °C
       Sample Temperature: 130 °C
       Reservoir, 75 eV
    

          28.0       5.3
          31.0       2.2
          37.0       2.1
          38.0       3.3
          39.0       4.9
          40.0       1.3
          41.0       4.4
          45.5       1.2
          50.0       2.0
          51.0       1.9
          52.0       4.0
          55.5       2.5
          56.0       1.3
          57.0       8.7
          58.0       1.3
          61.0       1.8
          62.0       2.4
          63.0       5.7
          64.0      10.0
          65.0       4.2
          70.0       1.2
          72.0       1.7
          75.0       1.7
          81.0       1.8
          82.0       1.8
          83.0      20.6
          84.0      32.0
          85.0       3.6
          90.0       1.5
          91.0       5.2
          94.0       1.3
         110.0       5.9
         111.0     100.0
         112.0       6.7
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6 H6 F N 0.05 ml : 0.5 ml CDCl3
    m-fluoroaniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.036 B 6.413 C 6.366 D 6.311 E 3.72 J(A,F-19)=6.7HZ J(A,B)=8.2HZ J(A,C)=8.0HZ J(A,D)=0.4HZ J(B,F-19)=8.8HZ J(B,C)=1.0HZ J(B,D)=2.4HZ J(C,D)=2.2HZ J(D,F-19)=11.0HZ

         Hz     ppm     Int.
    

       2823.73   7.066    428
       2823.36   7.065    397
       2820.68   7.058     33
       2816.77   7.049    480
       2815.43   7.045    846
       2808.84   7.029    839
       2807.50   7.025    581
       2807.13   7.024    531
       2803.96   7.017     34
       2803.71   7.016     34
       2802.86   7.014     34
       2800.54   7.008    514
       2573.36   6.440    392
       2572.51   6.437    420
       2570.92   6.433    435
       2570.07   6.431    472
       2567.87   6.426     48
       2567.02   6.424     53
       2565.19   6.419    376
       2564.58   6.418    500
       2564.21   6.417    528
       2563.72   6.415    479
       2562.74   6.413    477
       2562.13   6.411    567
       2561.77   6.411    587
       2561.28   6.409    531
       2557.86   6.401     54
       2556.27   6.397    361
       2555.42   6.395    435
       2553.83   6.391    402
       2552.98   6.389    488
       2550.05   6.381    739
       2549.07   6.379    744
       2547.85   6.376    917
       2546.88   6.373    852
       2543.95   6.366     75
       2541.99   6.361    753
       2541.14   6.359    707
       2539.79   6.356   1000
       2538.94   6.353    915
       2535.89   6.346     51
       2535.16   6.344     39
       2534.18   6.341     34
       2533.81   6.341     34
       2529.79   6.331    514
       2529.42   6.330    602
       2527.22   6.324    843
       2525.15   6.319    433
       2524.78   6.318    440
       2518.43   6.302    563
       2516.24   6.297    914
       2513.79   6.290    469
       1486.69   3.720    287
    


  • 1H NMR 89.56 MHz
    C6 H6 F N 0.02 ml : 0.5 ml CDCl3
    m-fluoroaniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.06 B 6.56 to 6.23 C 3.64

         Hz     ppm     Int.
    

        637.00   7.113    218
        636.63   7.109    227
        635.88   7.101    225
        629.38   7.028    291
        622.00   6.946    172
        621.44   6.939    176
        584.31   6.525    155
        583.38   6.514    173
        582.25   6.502    186
        576.00   6.432    754
        574.13   6.411    676
        571.13   6.378    358
        569.75   6.362    330
        568.63   6.350    295
        565.25   6.312    393
        562.94   6.286    304
        560.88   6.263    144
        325.88   3.639   1000
    

in CDCl3



liquid film





OXIDATION WITH PERBENZOIC ACID