-
MassMS-IW-9723 2,4,5-trifluoroaniline C6H4F3N (Mass of molecular ion: 147)
Source Temperature: 230 °C Sample Temperature: 150 °C Reservoir, 75 eV
28.0 6.3 31.0 5.4 46.0 1.0 50.0 3.9 51.0 5.3 52.0 2.6 56.0 2.3 57.0 2.3 61.0 1.3 63.5 1.1 68.0 1.4 69.0 4.6 70.0 7.5 73.5 7.5 74.0 1.6 75.0 6.4 76.0 3.8 77.0 1.7 80.0 1.9 81.0 4.0 82.0 1.2 93.0 1.2 94.0 1.5 96.0 1.4 99.0 7.1 100.0 25.3 101.0 7.8 103.0 1.0 107.0 2.7 108.0 1.0 116.0 2.8 118.0 1.0 119.0 25.1 120.0 22.3 121.0 1.3 126.0 4.4 127.0 11.5 128.0 1.7 130.0 1.4 146.0 5.1 147.0 100.0 148.0 7.0
400 MHz in CDCl3
-
1H NMR 399.65 MHz C6 H4 F3 N 0.041 g : 0.5 ml CDCl3 2,4,5-trifluoroaniline 
Assign. Shift(ppm)
A 6.867 B 6.583 C 3.66
Hz ppm Int.2758.54 6.903 550 2751.34 6.885 595 2748.17 6.877 996 2744.38 6.867 89 2740.97 6.859 1000 2738.04 6.852 574 2730.83 6.834 545 2644.65 6.618 557 2636.60 6.598 987 2633.42 6.590 582 2628.66 6.578 598 2625.24 6.569 980 2617.31 6.550 552 1461.91 3.658 463
in CDCl3
KBr disk
nujol mull
更多供应商
