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MS-IW-3594 p-(trifluoromethoxy)aniline C7H6F3NO (Mass of molecular ion: 177)
Source Temperature: 220 °C Sample Temperature: 160 °C Reservoir, 75 eV
26.0 1.0 27.0 2.0 28.0 3.1 38.0 1.5 39.0 3.4 41.0 1.5 46.0 1.1 50.0 1.6 51.0 2.9 52.0 9.1 53.0 11.3 54.0 2.8 62.0 1.6 63.0 3.3 64.0 1.5 65.0 4.3 69.0 10.3 78.0 1.2 79.0 2.7 80.0 31.4 81.0 2.1 83.0 2.4 90.0 1.0 92.0 12.7 101.0 1.1 108.0 98.3 109.0 7.4 110.0 1.1 149.0 2.5 176.0 3.2 177.0 100.0 178.0 8.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H6 F3 N O 0.05 ml : 0.5 ml CDCl3 p-(trifluoromethoxy)aniline Assign. Shift(ppm)
A 6.983 B 6.575 C 3.59
Hz ppm Int.
2798.95 7.004 61 2797.97 7.002 77 2795.53 6.995 453 2794.68 6.993 489 2793.70 6.991 323 2792.36 6.988 193 2788.82 6.979 187 2786.50 6.973 526 2785.64 6.971 522 2783.20 6.965 100 2782.23 6.962 79 2635.50 6.595 137 2632.08 6.586 1000 2629.76 6.581 375 2625.37 6.570 347 2623.05 6.564 919 2619.63 6.555 118 1434.57 3.590 289
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