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网站主页CAS数据库列表 3497-00-5更多图谱苯基硫代磷酰二氯(3497-00-5)核磁图(1HNMR)

苯基硫代磷酰二氯

产品名称 苯基硫代磷酰二氯

CAS号3497-00-5

分子式C6H5Cl2PS

分子量211.05

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  • Mass

    MS-IW-8107          
    phenylphosphonothioic dichloride
    C6H5Cl2PS           (Mass of molecular ion:    210)
    

       Source Temperature: 200 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          27.0       1.5
          38.0       1.0
          39.0       2.8
          50.0       8.6
          51.0      26.7
          52.0       1.5
          56.0       1.9
          57.0       1.6
          63.0      15.8
          65.0       4.8
          68.0       1.3
          69.0       2.8
          74.0       3.1
          75.0       3.0
          76.0       2.1
          77.0      33.9
          78.0       2.4
          80.0       2.5
          81.0       3.1
          82.0       1.1
          91.0       1.2
         101.0       2.6
         103.0       1.8
         107.0      10.1
         108.0       2.9
         109.0      94.7
         110.0       7.2
         111.0       4.8
         112.0       2.0
         139.0      28.1
         140.0       2.5
         141.0       2.1
         143.0      16.5
         144.0       1.2
         145.0       5.4
         174.0       1.0
         175.0      85.2
         176.0       6.7
         177.0      31.6
         178.0       3.7
         179.0       1.5
         180.0       1.0
         210.0     100.0
         211.0       7.6
         212.0      68.6
         213.0       5.1
         214.0      13.1
         215.0       1.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6 H5 Cl2 P S 0.05 ml : 0.5 ml CDCl3
    phenylphosphonothioic dichloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.113 B 7.623 C 7.549

         Hz     ppm     Int.
    

       3258.54   8.154     85
       3256.47   8.149    531
       3255.74   8.147    525
       3255.13   8.145    627
       3254.52   8.144    309
       3253.78   8.142    341
       3250.24   8.133    206
       3248.17   8.128    839
       3246.70   8.124    648
       3239.26   8.106     92
       3237.30   8.101    547
       3236.08   8.098    638
       3235.35   8.096    323
       3234.62   8.094    345
       3232.30   8.088     58
       3230.96   8.085    213
       3229.00   8.080    826
       3227.54   8.076    681
       3058.59   7.654     79
       3057.37   7.651    151
       3056.03   7.647    122
       3054.32   7.643    172
       3053.10   7.640    115
       3052.37   7.638    123
       3050.05   7.632    402
       3047.24   7.625    411
       3044.80   7.619    174
       3043.82   7.617    246
       3042.48   7.613    403
       3041.14   7.610    319
       3039.55   7.606    393
       3038.21   7.603    213
       3028.81   7.579    115
       3026.73   7.574    551
       3025.39   7.571    279
       3022.71   7.564    151
       3020.63   7.559    895
       3019.04   7.555   1000
       3014.28   7.543    477
       3012.94   7.539    864
       3012.33   7.538    645
       3010.86   7.534    380
       3007.32   7.525    170
       3005.62   7.521    348
       3004.64   7.519    255
    

in CDCl3



liquid film