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网站主页CAS数据库列表 644-97-3更多图谱苯基二氯化磷(644-97-3)核磁图(13CNMR)

苯基二氯化磷

产品名称 苯基二氯化磷

CAS号644-97-3

分子式C6H5Cl2P

分子量178.98

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  • Mass

    MS-NW-2642          
    dichloro(phenyl)phosphine
    C6H5Cl2P            (Mass of molecular ion:    178)
    

       Source Temperature: 280 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          27.0       1.4
          36.0       1.7
          38.0       1.0
          39.0       3.3
          50.0       5.8
          51.0      18.1
          52.0       1.0
          56.0       3.3
          57.0       2.8
          63.0       2.0
          66.0       1.1
          68.0       1.4
          69.0       1.2
          74.0       1.7
          75.0       1.7
          76.0       1.3
          77.0      30.9
          78.0       2.2
          80.0       3.1
          81.0       5.1
          82.0       1.4
          91.0       2.3
         101.0       1.4
         103.0       1.0
         107.0      27.1
         108.0       5.0
         112.0       1.3
         143.0     100.0
         144.0       6.8
         145.0      32.3
         146.0       3.1
         178.0      38.2
         179.0       2.7
         180.0      24.8
         181.0       1.6
         182.0       4.0
         224.0       1.0
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H5 Cl2 P 0.05 ml : 0.5 ml CDCl3
    dichloro(phenyl)phosphine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.88 B 7.53 C 7.50

         Hz     ppm     Int.
    

        715.94   7.994    291
        714.31   7.976    207
        713.56   7.968    364
        712.44   7.955     92
        711.38   7.944    209
        710.81   7.937    199
        709.88   7.927    430
        708.63   7.913    265
        707.50   7.900    310
        707.06   7.895    336
        706.38   7.888    458
        705.31   7.876    321
        704.63   7.868    448
        703.44   7.855    124
        702.31   7.842    234
        701.56   7.834    367
        701.19   7.830    260
        700.69   7.824    389
        699.63   7.812    271
        698.38   7.798    277
        697.38   7.787    446
        696.56   7.778    199
        695.38   7.765    101
        694.69   7.757     88
        685.06   7.650     77
        684.13   7.639     67
        682.63   7.623     66
        680.81   7.602    152
        680.06   7.594    143
        678.94   7.581    189
        678.13   7.572    166
        676.75   7.557    944
        675.75   7.546    456
        675.00   7.537   1000
        674.44   7.531    956
        674.00   7.526    636
        673.38   7.519    463
        672.81   7.513    711
        672.31   7.507    582
        672.00   7.504    419
        671.19   7.495    393
        670.06   7.482    771
        669.44   7.475    425
        668.25   7.462    451
        667.19   7.450     92
        666.44   7.442    204
        665.88   7.436     66
        665.56   7.432     92
        664.31   7.418    151
    

in CDCl3



liquid film





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