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MassMS-NW-2642 dichloro(phenyl)phosphine C6H5Cl2P (Mass of molecular ion: 178)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
27.0 1.4 36.0 1.7 38.0 1.0 39.0 3.3 50.0 5.8 51.0 18.1 52.0 1.0 56.0 3.3 57.0 2.8 63.0 2.0 66.0 1.1 68.0 1.4 69.0 1.2 74.0 1.7 75.0 1.7 76.0 1.3 77.0 30.9 78.0 2.2 80.0 3.1 81.0 5.1 82.0 1.4 91.0 2.3 101.0 1.4 103.0 1.0 107.0 27.1 108.0 5.0 112.0 1.3 143.0 100.0 144.0 6.8 145.0 32.3 146.0 3.1 178.0 38.2 179.0 2.7 180.0 24.8 181.0 1.6 182.0 4.0 224.0 1.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H5 Cl2 P 0.05 ml : 0.5 ml CDCl3 dichloro(phenyl)phosphine 
Assign. Shift(ppm)
A 7.88 B 7.53 C 7.50
Hz ppm Int.715.94 7.994 291 714.31 7.976 207 713.56 7.968 364 712.44 7.955 92 711.38 7.944 209 710.81 7.937 199 709.88 7.927 430 708.63 7.913 265 707.50 7.900 310 707.06 7.895 336 706.38 7.888 458 705.31 7.876 321 704.63 7.868 448 703.44 7.855 124 702.31 7.842 234 701.56 7.834 367 701.19 7.830 260 700.69 7.824 389 699.63 7.812 271 698.38 7.798 277 697.38 7.787 446 696.56 7.778 199 695.38 7.765 101 694.69 7.757 88 685.06 7.650 77 684.13 7.639 67 682.63 7.623 66 680.81 7.602 152 680.06 7.594 143 678.94 7.581 189 678.13 7.572 166 676.75 7.557 944 675.75 7.546 456 675.00 7.537 1000 674.44 7.531 956 674.00 7.526 636 673.38 7.519 463 672.81 7.513 711 672.31 7.507 582 672.00 7.504 419 671.19 7.495 393 670.06 7.482 771 669.44 7.475 425 668.25 7.462 451 667.19 7.450 92 666.44 7.442 204 665.88 7.436 66 665.56 7.432 92 664.31 7.418 151
in CDCl3
liquid film
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