4,4'-联苯二磺酰氯

产品名称 4,4'-联苯二磺酰氯

CAS号3406-84-6

分子式C12H8Cl2O4S2

分子量351.23

¹³CNMR

Mass

MS-NW-6211          
4,4'-biphenyldisulfonyl dichloride
C12H8Cl2O4S2        (Mass of molecular ion:    350)

   Source Temperature: 180 °C
   Sample Temperature: 180 °C
   Direct, 75 eV

      18.0       4.5
      27.0       1.2
      28.0       1.4
      35.0       1.2
      36.0       7.6
      38.0       2.5
      39.0       2.6
      48.0       4.6
      50.0       5.3
      51.0       4.6
      62.0       3.0
      63.0      13.3
      63.5       1.1
      64.0       9.2
      69.0       1.1
      74.0       4.3
      75.0       8.1
      75.5       2.4
      76.0      32.1
      76.5       3.9
      77.0       2.5
      86.0       1.7
      87.0       2.6
      88.0       1.0
      89.0       1.3
      91.0       1.0
      98.0       1.6
      99.0       1.9
     100.0       2.7
     101.0       2.1
     102.0       3.2
     108.0       5.5
     111.0       1.4
     113.0       1.8
     114.0       1.1
     125.0       2.3
     126.0       7.6
     127.0       1.4
     139.0       5.8
     140.0       3.6
     149.0       1.2
     150.0      10.1
     151.0      29.4
     152.0     100.0
     153.0      14.0
     154.0       1.6
     167.0       1.5
     168.0       2.9
     186.0       1.4
     187.0       2.5
     188.0       2.1
     200.0       1.8
     216.0       1.5
     251.0      37.7
     252.0       5.8
     253.0      14.4
     254.0       2.3
     267.0       1.5
     299.0       1.5
     315.0      49.5
     316.0       7.6
     317.0      22.0
     318.0       3.4
     319.0       2.1
     350.0      28.8
     351.0       4.5
     352.0      22.0
     353.0       3.4
     354.0       5.2

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₂ H₈ Cl₂ O₄ S₂	0.040 g : 0.5 ml DMSO-d₆
4,4'-biphenyldisulfonyl dichloride

    Assign.     Shift(ppm)

      A     *1      7.747
      B     *1      7.690

     Hz     ppm     Int.

   3101.62   7.761    513
   3093.50   7.741   1000
   3076.41   7.698    934
   3068.08   7.677    508

in DMSO-d6

KBr disc

nujol mull

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4,4'-联苯二磺酰氯(3406-84-6)质谱(MS) 相关产品图谱

4,4'-联苯二磺酰氯(3406-84-6)质谱(MS) 4,4'-联苯二磺酰氯(3406-84-6)核磁图(¹³CNMR) 4,4'-联苯二磺酰氯(3406-84-6)核磁图(¹HNMR) 4,4'-联苯二磺酰氯(3406-84-6)红外图谱(IR1) 4,4'-联苯二磺酰氯(3406-84-6)红外图谱(IR2)

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