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网站主页CAS数据库列表 1622-32-8更多图谱2-氯乙烷磺酰氯(1622-32-8)核磁图(1HNMR)

2-氯乙烷磺酰氯

产品名称 2-氯乙烷磺酰氯

CAS号1622-32-8

分子式C2H4Cl2O2S

分子量163.02

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  • Mass

    MS-IW-3818          
    2-chloro-1-ethanesulfonyl chloride
    C2H4Cl2O2S          (Mass of molecular ion:    162)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          26.0       7.9
          27.0      63.3
          28.0       9.3
          32.0       1.1
          35.0       1.4
          36.0       5.2
          38.0       1.8
          44.0       1.2
          45.0       1.5
          48.0       7.0
          49.0       3.0
          57.0       1.0
          58.0       1.1
          61.0       3.2
          62.0      13.1
          63.0     100.0
          64.0      13.4
          65.0      36.9
          66.0       1.4
          83.0       2.8
          85.0       1.0
          91.0      27.3
          93.0       1.4
          99.0       1.5
         127.0       6.4
         129.0       2.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C2 H4 Cl2 O2 S 0.05 ml : 0.5 ml CDCl3
    2-chloro-1-ethanesulfonyl chloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 4.088 B *1 4.007

         Hz     ppm     Int.
    

       1643.07   4.112    408
       1641.24   4.107    450
       1637.42   4.098    209
       1636.51   4.095    523
       1634.98   4.092    953
       1633.45   4.088    615
       1630.86   4.081    212
       1628.27   4.075   1000
       1625.52   4.068    372
       1610.11   4.029    374
       1607.51   4.023    979
       1604.61   4.016    214
       1602.17   4.009    585
       1600.65   4.006    946
       1599.12   4.002    510
       1598.05   3.999    213
       1594.24   3.990    459
       1592.56   3.985    403
       1587.98   3.974     26
    

in CDCl3



liquid film