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MS-IW-3818 2-chloro-1-ethanesulfonyl chloride C2H4Cl2O2S (Mass of molecular ion: 162)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
26.0 7.9 27.0 63.3 28.0 9.3 32.0 1.1 35.0 1.4 36.0 5.2 38.0 1.8 44.0 1.2 45.0 1.5 48.0 7.0 49.0 3.0 57.0 1.0 58.0 1.1 61.0 3.2 62.0 13.1 63.0 100.0 64.0 13.4 65.0 36.9 66.0 1.4 83.0 2.8 85.0 1.0 91.0 27.3 93.0 1.4 99.0 1.5 127.0 6.4 129.0 2.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C2 H4 Cl2 O2 S 0.05 ml : 0.5 ml CDCl3 2-chloro-1-ethanesulfonyl chloride Assign. Shift(ppm)
A *1 4.088 B *1 4.007
Hz ppm Int.
1643.07 4.112 408 1641.24 4.107 450 1637.42 4.098 209 1636.51 4.095 523 1634.98 4.092 953 1633.45 4.088 615 1630.86 4.081 212 1628.27 4.075 1000 1625.52 4.068 372 1610.11 4.029 374 1607.51 4.023 979 1604.61 4.016 214 1602.17 4.009 585 1600.65 4.006 946 1599.12 4.002 510 1598.05 3.999 213 1594.24 3.990 459 1592.56 3.985 403 1587.98 3.974 26
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