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MassMS-IW-0822 cyclopropyldiphenylsulfonium tetrafluoroborate C15H15BF4S (Mass of molecular ion: 314)
Source Temperature: 180 °C Sample Temperature: 170 °C Direct, 75 eV
18.0 2.2 20.0 1.1 27.0 1.4 39.0 7.8 40.0 1.8 41.0 2.8 45.0 1.9 48.0 2.4 49.0 9.5 50.0 1.7 51.0 8.6 59.0 7.6 60.0 4.8 63.0 1.9 65.0 5.5 66.0 1.5 68.0 1.0 69.0 2.7 76.0 1.1 77.0 9.4 78.0 2.3 79.0 1.9 89.0 2.3 91.0 5.6 92.0 5.3 93.0 1.8 99.0 1.5 102.0 1.6 103.0 1.5 105.0 1.9 108.0 1.3 109.0 4.7 110.0 1.7 115.0 21.5 116.0 9.8 117.0 9.7 121.0 2.3 134.0 8.9 135.0 7.4 136.0 1.0 139.0 1.8 141.0 2.3 142.0 1.1 147.0 9.1 148.0 3.3 149.0 32.2 150.0 5.2 151.0 3.0 152.0 7.8 153.0 3.8 154.0 1.5 165.0 3.5 166.0 1.0 167.0 1.8 171.0 4.1 178.0 9.7 179.0 1.7 183.0 1.4 184.0 29.7 185.0 70.8 186.0 100.0 187.0 16.3 188.0 5.3 197.0 8.2 198.0 1.4 199.0 1.1 210.0 2.5 211.0 50.7 212.0 8.4 213.0 2.9 225.0 3.8 226.0 49.6 227.0 9.4 228.0 3.0
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C15 H15 B F4 S 0.032 g : 0.5 ml DMSO-d6 cyclopropyldiphenylsulfonium tetrafluoroborate 
Assign. Shift(ppm)
A 8.062 B 7.833 C 7.787 D 3.927 E *1 1.621 F *1 1.529
Hz ppm Int.3229.06 8.080 84 3226.32 8.073 610 3225.71 8.072 579 3225.10 8.070 672 3224.33 8.068 329 3223.57 8.066 374 3220.21 8.058 241 3218.08 8.053 1000 3216.71 8.049 671 3141.94 7.862 75 3140.72 7.859 139 3139.34 7.856 96 3136.14 7.848 104 3133.24 7.840 469 3130.95 7.835 159 3127.44 7.826 304 3126.07 7.823 497 3124.69 7.819 245 3122.86 7.814 53 3120.12 7.808 141 3118.13 7.803 558 3117.52 7.801 714 3116.00 7.797 308 3111.72 7.787 392 3109.89 7.782 795 3108.06 7.777 180 3107.15 7.775 126 3104.55 7.769 166 3102.87 7.764 330 3101.35 7.761 189 3100.43 7.758 92 1581.57 3.958 32 1577.45 3.948 73 1574.25 3.940 84 1569.98 3.929 154 1565.70 3.918 89 1562.50 3.910 81 1558.23 3.899 39 658.57 1.648 34 657.35 1.645 45 653.08 1.635 114 652.01 1.632 117 650.18 1.627 190 649.41 1.625 185 648.04 1.622 214 645.29 1.615 221 643.92 1.612 156 640.87 1.604 91 639.65 1.601 65 634.46 1.588 35 630.04 1.577 34 627.29 1.570 34 625.61 1.566 34 620.73 1.554 75 619.35 1.550 68 616.46 1.543 109 614.32 1.538 183 613.25 1.535 175 612.34 1.533 156 608.98 1.524 123 606.99 1.519 192 605.01 1.514 122 599.67 1.501 42 598.45 1.498 39
in DMSO-d6
KBr disc
nujol mull
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