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网站主页CAS数据库列表 33462-81-6更多图谱环丙基二苯基锍四氟硼酸盐(33462-81-6)核磁图(1HNMR)

环丙基二苯基锍四氟硼酸盐

产品名称 环丙基二苯基锍四氟硼酸盐

CAS号33462-81-6

分子式C15H15BF4S

分子量314.15

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  • Mass

    MS-IW-0822          
    cyclopropyldiphenylsulfonium tetrafluoroborate
    C15H15BF4S          (Mass of molecular ion:    314)
    

       Source Temperature: 180 °C
       Sample Temperature: 170 °C
       Direct, 75 eV
    

          18.0       2.2
          20.0       1.1
          27.0       1.4
          39.0       7.8
          40.0       1.8
          41.0       2.8
          45.0       1.9
          48.0       2.4
          49.0       9.5
          50.0       1.7
          51.0       8.6
          59.0       7.6
          60.0       4.8
          63.0       1.9
          65.0       5.5
          66.0       1.5
          68.0       1.0
          69.0       2.7
          76.0       1.1
          77.0       9.4
          78.0       2.3
          79.0       1.9
          89.0       2.3
          91.0       5.6
          92.0       5.3
          93.0       1.8
          99.0       1.5
         102.0       1.6
         103.0       1.5
         105.0       1.9
         108.0       1.3
         109.0       4.7
         110.0       1.7
         115.0      21.5
         116.0       9.8
         117.0       9.7
         121.0       2.3
         134.0       8.9
         135.0       7.4
         136.0       1.0
         139.0       1.8
         141.0       2.3
         142.0       1.1
         147.0       9.1
         148.0       3.3
         149.0      32.2
         150.0       5.2
         151.0       3.0
         152.0       7.8
         153.0       3.8
         154.0       1.5
         165.0       3.5
         166.0       1.0
         167.0       1.8
         171.0       4.1
         178.0       9.7
         179.0       1.7
         183.0       1.4
         184.0      29.7
         185.0      70.8
         186.0     100.0
         187.0      16.3
         188.0       5.3
         197.0       8.2
         198.0       1.4
         199.0       1.1
         210.0       2.5
         211.0      50.7
         212.0       8.4
         213.0       2.9
         225.0       3.8
         226.0      49.6
         227.0       9.4
         228.0       3.0
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C15 H15 B F4 S 0.032 g : 0.5 ml DMSO-d6
    cyclopropyldiphenylsulfonium tetrafluoroborate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.062 B 7.833 C 7.787 D 3.927 E *1 1.621 F *1 1.529

         Hz     ppm     Int.
    

       3229.06   8.080     84
       3226.32   8.073    610
       3225.71   8.072    579
       3225.10   8.070    672
       3224.33   8.068    329
       3223.57   8.066    374
       3220.21   8.058    241
       3218.08   8.053   1000
       3216.71   8.049    671
       3141.94   7.862     75
       3140.72   7.859    139
       3139.34   7.856     96
       3136.14   7.848    104
       3133.24   7.840    469
       3130.95   7.835    159
       3127.44   7.826    304
       3126.07   7.823    497
       3124.69   7.819    245
       3122.86   7.814     53
       3120.12   7.808    141
       3118.13   7.803    558
       3117.52   7.801    714
       3116.00   7.797    308
       3111.72   7.787    392
       3109.89   7.782    795
       3108.06   7.777    180
       3107.15   7.775    126
       3104.55   7.769    166
       3102.87   7.764    330
       3101.35   7.761    189
       3100.43   7.758     92
       1581.57   3.958     32
       1577.45   3.948     73
       1574.25   3.940     84
       1569.98   3.929    154
       1565.70   3.918     89
       1562.50   3.910     81
       1558.23   3.899     39
        658.57   1.648     34
        657.35   1.645     45
        653.08   1.635    114
        652.01   1.632    117
        650.18   1.627    190
        649.41   1.625    185
        648.04   1.622    214
        645.29   1.615    221
        643.92   1.612    156
        640.87   1.604     91
        639.65   1.601     65
        634.46   1.588     35
        630.04   1.577     34
        627.29   1.570     34
        625.61   1.566     34
        620.73   1.554     75
        619.35   1.550     68
        616.46   1.543    109
        614.32   1.538    183
        613.25   1.535    175
        612.34   1.533    156
        608.98   1.524    123
        606.99   1.519    192
        605.01   1.514    122
        599.67   1.501     42
        598.45   1.498     39
    

in DMSO-d6



KBr disc



nujol mull