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MS-NW-6313 5-indanamine C9H11N (Mass of molecular ion: 133)
Source Temperature: 270 °C Sample Temperature: 190 °C Reservoir, 75 eV
27.0 2.0 28.0 2.2 30.0 1.1 39.0 4.0 41.0 1.2 50.0 1.9 51.0 4.6 52.0 2.9 53.0 1.9 54.0 1.9 62.0 1.0 63.0 2.4 64.5 2.7 65.0 6.3 65.5 7.0 66.0 2.7 66.5 1.9 76.0 1.0 77.0 6.5 78.0 2.6 79.0 2.7 89.0 1.4 91.0 2.7 93.0 1.2 102.0 1.1 103.0 3.6 104.0 3.4 105.0 4.8 106.0 4.8 115.0 10.1 116.0 2.5 117.0 10.6 118.0 2.3 130.0 9.5 131.0 5.9 132.0 100.0 133.0 77.7 134.0 7.8
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H11 N 0.040 g : 0.5 ml CDCl3 5-indanamine Assign. Shift(ppm)
A 6.982 B 6.571 C 6.474 D 3.48 E 2.789 F 2.303
Hz ppm Int.
630.00 7.035 143 622.25 6.948 188 621.81 6.943 184 589.56 6.583 160 589.13 6.579 157 588.06 6.567 220 587.50 6.560 218 584.00 6.521 212 582.50 6.505 87 581.75 6.496 110 576.19 6.434 140 574.63 6.417 71 573.94 6.409 103 312.13 3.486 1000 258.31 2.885 155 257.38 2.874 171 250.94 2.802 463 246.75 2.756 64 243.94 2.724 275 243.19 2.716 273 195.44 2.183 84 194.13 2.168 94 188.56 2.106 159 187.25 2.091 235 184.63 2.062 47 181.75 2.030 95 180.25 2.013 328 173.25 1.935 220 171.50 1.915 50
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