400 MHz in CDCl3
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1H NMR 399.65 MHz C32 H68 Br P 0.043 g : 0.5 ml CDCl3 tetraoctylphosphonium bromide Assign. Shift(ppm)
A 2.450 B 1.55 C 1.51 D 1.32 to 1.27 E 0.881
Hz ppm Int.
993.90 2.487 81 987.43 2.471 93 981.08 2.455 133 977.78 2.447 145 964.60 2.414 108 633.91 1.587 64 632.32 1.583 61 625.98 1.567 110 624.51 1.563 109 617.68 1.546 130 613.53 1.536 110 609.62 1.526 155 603.76 1.511 185 596.56 1.493 156 596.31 1.493 156 590.33 1.478 105 588.75 1.474 108 581.91 1.457 50 527.34 1.320 236 519.53 1.300 342 515.50 1.290 403 512.70 1.283 431 509.40 1.275 554 506.47 1.268 487 359.25 0.899 319 352.54 0.883 1000 345.58 0.865 374
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