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四丁基氯化膦

CAS号2304-30-5

分子式C16H36ClP

分子量294.88

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  • Mass

    MS-IW-9005          
    tetrabutylphosphonium chloride
    C16H36ClP           (Mass of molecular ion:    294)
    

       Source Temperature: 200 °C
       Sample Temperature: 230 °C
       Direct, 75 eV
    

          18.0       2.0
          25.0       1.1
          26.0       8.0
          27.0      22.0
          28.0      21.6
          29.0      34.9
          35.0       4.2
          36.0      35.6
          37.0       2.2
          38.0      12.9
          39.0      19.7
          40.0       3.4
          41.0      55.4
          42.0       5.6
          43.0       9.6
          44.0       1.3
          45.0       6.1
          46.0       1.5
          47.0       6.0
          48.0       7.3
          49.0       2.8
          50.0       3.0
          51.0       3.0
          52.0       1.6
          53.0       8.0
          54.0       7.9
          55.0      39.9
          56.0      13.7
          57.0      14.8
          58.0       3.7
          59.0      13.1
          60.0       4.9
          61.0      37.0
          62.0      65.3
          63.0       3.5
          67.0       2.3
          68.0       1.3
          69.0       9.3
          71.0       6.0
          72.0       1.4
          73.0      10.1
          74.0      10.0
          75.0      11.1
          76.0      96.2
          77.0       4.2
          78.0       1.3
          79.0       1.0
          81.0       1.4
          83.0       4.3
          85.0       3.7
          86.0       2.1
          87.0       8.6
          88.0      13.9
          89.0      29.9
          90.0      17.9
          91.0       3.1
          92.0       1.2
          96.0       1.3
          97.0       1.7
          99.0       1.3
         100.0       1.5
         101.0       4.5
         102.0      10.5
         103.0      22.9
         104.0      37.3
         105.0       4.0
         113.0       1.0
         114.0       1.1
         115.0       5.7
         116.0       6.8
         117.0      10.2
         118.0      40.7
         119.0       3.1
         129.0       3.7
         130.0       3.7
         131.0      18.8
         132.0       6.2
         143.0       3.3
         144.0       3.2
         145.0      30.8
         146.0      26.5
         147.0       4.0
         157.0       2.5
         158.0       1.6
         159.0       4.5
         160.0      17.5
         161.0       2.1
         171.0       4.2
         172.0       1.2
         173.0      33.6
         174.0       5.9
         185.0       1.4
         187.0       7.7
         188.0       1.1
         199.0       3.0
         200.0       1.7
         201.0      62.5
         202.0      30.5
         203.0       4.9
         213.0       1.1
         215.0       1.7
         227.0       3.7
         229.0     100.0
         230.0      15.9
         231.0       1.4
         243.0       2.4
         243.5       2.3
         257.0      22.2
         258.0      17.7
         259.0      91.4
         260.0      16.0
         261.0       1.3
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C16 H36 Cl P 0.05 ml : 0.5 ml DMSO-d6
    tetrabutylphosphonium chloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.266 B 1.47 C 1.42 D 0.920

         Hz     ppm     Int.
    

        921.75   2.307     96
        914.67   2.289    103
        911.38   2.281     94
        908.20   2.273    152
        905.64   2.267    166
        903.08   2.260    105
        900.88   2.255    106
        891.85   2.232    124
        603.64   1.511     76
        601.44   1.505     72
        595.95   1.492    129
        594.12   1.487    129
        587.04   1.469    150
        580.44   1.453    171
        577.03   1.444    149
        574.34   1.438    207
        567.38   1.420    219
        560.42   1.403    181
        553.10   1.384     94
        546.51   1.368     31
        374.39   0.937    524
        367.43   0.920   1000
        360.11   0.902    395
    

in DMSO-d6



liquid film