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MassMS-NW-7420 tetraphenylphosphonium bromide C24H20BrP (Mass of molecular ion: 418)
Source Temperature: 190 °C Sample Temperature: 300 °C Direct, 75 eV
18.0 3.5 27.0 1.0 39.0 4.2 50.0 4.4 51.0 11.3 52.0 3.2 57.0 3.4 63.0 2.5 65.0 2.2 74.0 1.7 75.0 1.3 76.0 1.8 77.0 7.9 78.0 12.8 79.0 2.7 80.0 6.2 81.0 3.0 82.0 6.4 83.0 1.6 89.0 1.1 91.0 1.0 102.0 1.1 107.0 16.7 108.0 38.8 109.0 3.5 115.0 4.5 128.0 1.6 131.0 2.2 133.0 3.9 139.0 2.1 141.0 1.8 151.0 1.3 152.0 9.9 153.0 3.4 154.0 4.4 157.0 4.8 170.0 3.2 181.0 1.9 182.0 1.1 183.0 76.7 184.0 16.4 185.0 11.9 186.0 1.6 228.0 1.1 230.0 1.2 257.0 1.6 259.0 2.6 260.0 2.9 261.0 18.9 262.0 100.0 263.0 19.9 264.0 1.9 337.0 3.5 338.0 6.0 339.0 26.5 340.0 7.1 341.0 1.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C24 H20 Br P 0.040 g : 0.5 ml CDCl3 tetraphenylphosphonium bromide 
Assign. Shift(ppm)
A 7.949 B 7.835 C 7.650
Hz ppm Int.3187.01 7.975 243 3185.79 7.972 215 3184.94 7.970 263 3183.72 7.967 171 3181.40 7.961 179 3179.44 7.956 576 3177.49 7.951 614 3175.66 7.947 247 3173.22 7.940 260 3172.00 7.937 442 3171.14 7.935 382 3170.65 7.934 369 3169.92 7.932 470 3168.58 7.929 254 3142.09 7.863 134 3140.26 7.858 544 3139.65 7.857 393 3138.67 7.854 375 3136.72 7.849 583 3135.99 7.847 428 3135.13 7.845 387 3133.91 7.842 444 3133.42 7.841 524 3132.32 7.838 975 3130.37 7.833 556 3129.76 7.832 578 3128.66 7.829 949 3127.32 7.826 438 3124.76 7.819 566 3124.15 7.818 470 3123.05 7.815 325 3121.22 7.810 517 3120.61 7.809 423 3069.70 7.681 153 3067.87 7.677 740 3067.38 7.676 715 3066.77 7.674 955 3065.92 7.672 516 3064.94 7.670 371 3061.52 7.661 246 3059.45 7.656 860 3058.23 7.653 763 3056.64 7.649 262 3054.93 7.645 764 3054.32 7.643 710 3053.71 7.641 1000 3052.86 7.639 524 3048.46 7.628 251 3046.39 7.623 837 3045.17 7.620 758
in CDCl3
KBr disc
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